(R)-1-tritylethanol

Base Information

Chemical Name:(R)-1-tritylethanol
CAS No.:139164-44-6
Molecular Formula:C₂₁H₂₀O
Molecular Weight:288.389
Hs Code.:

Synonyms:(R)-1-tritylethanol

Suppliers and Price of (R)-1-tritylethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-1-tritylethanol

Chemical Property:

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Technology Process of (R)-1-tritylethanol

There total 6 articles about (R)-1-tritylethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 795-36-8
1,1,1-triphenylacetone

: 139164-44-6
(R)-1-tritylethanol

Guidance literature:: With borane-THF; oxazaborolidine 1 (R=Me); In toluene; for 0.333333h; Heating;
DOI:10.1016/0040-4039(91)80419-7

Reference yield:

: 795-36-8
1,1,1-triphenylacetone

: 139164-44-6
(R)-1-tritylethanol

: (S)-1,1,1-Triphenyl-propan-2-ol

Guidance literature:: With sodium tetrahydroborate; chloro-trimethyl-silane; polymer-supported chiral sulfonamide; In tetrahydrofuran; Title compound not separated from byproducts; Heating;
DOI:10.1002/1521-3773(20010316)40:6<1109::AID-ANIE11090>3.0.CO;2-T

Reference yield:

: 519-73-3
triphenylmethane

: 139164-44-6
(R)-1-tritylethanol

: (S)-1,1,1-Triphenyl-propan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1.75 h / -30 - 20 °C

1.2: 0.67 h / -78 °C

2.1: chromium(VI) oxide; sulfuric acid / water; acetone / 0 °C

3.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / toluene / 80 °C / Inert atmosphere

With chromium(VI) oxide; n-butyllithium; borane-THF; sulfuric acid; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; hexane; water; acetone; toluene; 3.1: |Corey-Bakshi-Shibata Reduction;
DOI:10.3390/molecules25030707