Technology Process of C29H34O4Si
There total 5 articles about C29H34O4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,6-dimethylpyridine;
In
1,3,5-trimethyl-benzene;
at 165 ℃;
for 8h;
DOI:10.1039/c1cc11758k
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / 0 °C
2: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 12 h / 20 °C / Molecular sieve
3: tert.-butyl lithium / diethyl ether / -78 °C
4: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / Molecular sieve
5: 2,6-dimethylpyridine / 1,3,5-trimethyl-benzene / 8 h / 165 °C
With
2,6-dimethylpyridine; lithium aluminium tetrahydride; tetrapropylammonium perruthennate; tert.-butyl lithium; 4-methylmorpholine N-oxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; 1,3,5-trimethyl-benzene;
DOI:10.1039/c1cc11758k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tert.-butyl lithium / diethyl ether / -78 °C
2: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / Molecular sieve
3: 2,6-dimethylpyridine / 1,3,5-trimethyl-benzene / 8 h / 165 °C
With
2,6-dimethylpyridine; tetrapropylammonium perruthennate; tert.-butyl lithium; 4-methylmorpholine N-oxide;
In
diethyl ether; dichloromethane; 1,3,5-trimethyl-benzene;
DOI:10.1039/c1cc11758k
