methyl 2-{[2-amino-4-(2-methoxy-2-oxoethyl)phenyl]amino}-4-chlorobenzoate

Base Information

Chemical Name:methyl 2-{[2-amino-4-(2-methoxy-2-oxoethyl)phenyl]amino}-4-chlorobenzoate
CAS No.:755026-47-2
Molecular Formula:C₁₇H₁₇ClN₂O₄
Molecular Weight:348.786
Hs Code.:

Synonyms:methyl 2-{[2-amino-4-(2-methoxy-2-oxoethyl)phenyl]amino}-4-chlorobenzoate

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Chemical Property of methyl 2-{[2-amino-4-(2-methoxy-2-oxoethyl)phenyl]amino}-4-chlorobenzoate

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Technology Process of methyl 2-{[2-amino-4-(2-methoxy-2-oxoethyl)phenyl]amino}-4-chlorobenzoate

There total 3 articles about methyl 2-{[2-amino-4-(2-methoxy-2-oxoethyl)phenyl]amino}-4-chlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 755026-46-1
methyl 4-chloro-2-{[4-(2-methoxy-2-oxoethyl)-2-nitrophenyl]amino}benzoate

: 755026-47-2
methyl 2-{[2-amino-4-(2-methoxy-2-oxoethyl)phenyl]amino}-4-chlorobenzoate

Guidance literature:: With hydrogen; platinum on carbon; In methanol; ethyl acetate; at 20 ℃;

Reference yield:

: 28694-94-2
methyl 2-(4-amino-3-nitrophenyl)acetate

: 755026-47-2
methyl 2-{[2-amino-4-(2-methoxy-2-oxoethyl)phenyl]amino}-4-chlorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / dppf; Cs₂CO₃ / Pd(OAc)2 / 16 h / 95 °C

2: H₂ / Pt/C / methanol / 20 °C

With 1,1'-bis-(diphenylphosphino)ferrocene; hydrogen; caesium carbonate; palladium diacetate; platinum on activated charcoal; In methanol;
DOI:10.1021/jm070105d

Reference yield:

: 181765-85-5
methyl 2-iodo 4-chlorobenzoate

: 755026-47-2
methyl 2-{[2-amino-4-(2-methoxy-2-oxoethyl)phenyl]amino}-4-chlorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / dppf; Cs₂CO₃ / Pd(OAc)2 / 16 h / 95 °C

2: H₂ / Pt/C / methanol / 20 °C

With 1,1'-bis-(diphenylphosphino)ferrocene; hydrogen; caesium carbonate; palladium diacetate; platinum on activated charcoal; In methanol;
DOI:10.1021/jm070105d