[(R)-Azido-(3-trifluoromethyl-phenyl)-methyl]-phosphonic acid diallyl ester

Base Information

Chemical Name:[(R)-Azido-(3-trifluoromethyl-phenyl)-methyl]-phosphonic acid diallyl ester
CAS No.:614754-46-0
Molecular Formula:C₁₄H₁₅F₃N₃O₃P
Molecular Weight:361.26
Hs Code.:

Synonyms:[(R)-Azido-(3-trifluoromethyl-phenyl)-methyl]-phosphonic acid diallyl ester

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Chemical Property of [(R)-Azido-(3-trifluoromethyl-phenyl)-methyl]-phosphonic acid diallyl ester

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Technology Process of [(R)-Azido-(3-trifluoromethyl-phenyl)-methyl]-phosphonic acid diallyl ester

There total 1 articles about [(R)-Azido-(3-trifluoromethyl-phenyl)-methyl]-phosphonic acid diallyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 536739-10-3
[(S)-Hydroxy-(3-trifluoromethyl-phenyl)-methyl]-phosphonic acid diallyl ester

: 614754-46-0
[(R)-Azido-(3-trifluoromethyl-phenyl)-methyl]-phosphonic acid diallyl ester

Guidance literature:: With tris-(2-chloro-ethyl)-amine; triphenylphosphine; diethylazodicarboxylate; at 0 - 20 ℃; for 20h;
DOI:10.1016/S0960-894X(03)00672-3

Reference yield:

: 614754-46-0
[(R)-Azido-(3-trifluoromethyl-phenyl)-methyl]-phosphonic acid diallyl ester

: [(R)-Amino-(3-trifluoromethyl-phenyl)-methyl]-phosphonic acid diallyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 2 h / 20 °C

2: H₂O / benzene / 5 h / 50 - 55 °C

With water; In benzene; 1: Staudinger reaction;
DOI:10.1016/S0960-894X(03)00672-3