1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carbonitrile

Base Information

Chemical Name:1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carbonitrile
CAS No.:117138-52-0
Molecular Formula:C₁₉H₁₄N₂O
Molecular Weight:286.333
Hs Code.:

1-benzoyl-1,2,2a,3-tetrahydrobenz<cd>indole-5-carbonitrile

Synonyms:1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carbonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carbonitrile

Chemical Property:

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Technology Process of 1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carbonitrile

There total 3 articles about 1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 117138-51-9
Phosphoric acid 1-benzoyl-5-cyano-1,2,2a,3,4,5-hexahydro-benzo[cd]indol-5-yl ester diethyl ester

: 117138-52-0
1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carbonitrile

Guidance literature:: With boron trifluoride diethyl etherate; In benzene; for 1.5h; Ambient temperature;
DOI:10.1248/cpb.35.4793

Reference yield:

: 117138-52-0
1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carbonitrile

Guidance literature:: With thionyl chloride; benzene;
DOI:10.1021/ja01594a039

Reference yield:

: 132008-45-8,51867-02-8
1-benzoyl-2,2a,3,4-tetrahydro-1H-benz[cd]indol-5-one

: 117138-52-0
1-benzoyl-1,2,2a,3-tetrahydrobenzindole-5-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: LiCN / tetrahydrofuran / 0.5 h / Ambient temperature

2: 90 percent / BF₃*Et₂O / benzene / 1.5 h / Ambient temperature

With boron trifluoride diethyl etherate; lithium cyanide; In tetrahydrofuran; benzene;
DOI:10.1248/cpb.35.4793