Technology Process of C23H28O3S2
There total 8 articles about C23H28O3S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride;
In
tetrahydrofuran;
for 6h;
Heating;
DOI:10.1016/j.tet.2003.08.059
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: NaH / tetrahydrofuran / 0 - 20 °C
1.2: 85 percent / p-toluenesulfonic acid / benzene / 8 h / Heating
2.1: 75 percent / HCOONH4 / Pd-C / ethanol / 6 h / Heating
3.1: 90 percent / BF3*(C2H5)2O / diethyl ether / 10 h / 0 - 20 °C
4.1: 94 percent / diethyl ether / 4 h / Heating
5.1: 70 percent / NaH; HMPA / tetrahydrofuran / 6 h / Heating
With
N,N,N,N,N,N-hexamethylphosphoric triamide; boron trifluoride diethyl etherate; ammonium formate; sodium hydride;
palladium on activated charcoal;
In
tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1016/j.tet.2003.08.059
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 90 percent / K2CO3 / acetone / 6 h / Heating
2.1: NaH / tetrahydrofuran / 0 - 20 °C
2.2: 85 percent / p-toluenesulfonic acid / benzene / 8 h / Heating
3.1: 75 percent / HCOONH4 / Pd-C / ethanol / 6 h / Heating
4.1: 90 percent / BF3*(C2H5)2O / diethyl ether / 10 h / 0 - 20 °C
5.1: 94 percent / diethyl ether / 4 h / Heating
6.1: 70 percent / NaH; HMPA / tetrahydrofuran / 6 h / Heating
With
N,N,N,N,N,N-hexamethylphosphoric triamide; boron trifluoride diethyl etherate; ammonium formate; sodium hydride; potassium carbonate;
palladium on activated charcoal;
In
tetrahydrofuran; diethyl ether; ethanol; acetone;
DOI:10.1016/j.tet.2003.08.059
