N-phenylmethyl-N'-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)butanediamide

Base Information

Chemical Name:N-phenylmethyl-N'-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)butanediamide
CAS No.:1000278-27-2
Molecular Formula:C₂₅H₃₂N₂O₁₁
Molecular Weight:536.536
Hs Code.:

Synonyms:N-phenylmethyl-N'-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)butanediamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenylmethyl-N'-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)butanediamide

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Technology Process of N-phenylmethyl-N'-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)butanediamide

There total 3 articles about N-phenylmethyl-N'-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)butanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1154040-96-6
N-benzyl-N'-(β-D-glucopyranosyl)succinamide

: 75-36-5
acetyl chloride

: 1000278-27-2
N-phenylmethyl-N'-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)butanediamide

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 12h;
DOI:10.1021/jo900532e

Reference yield: 69.0%

: 3194-60-3
thiolane-2,5-dione

: 41355-50-4,51642-81-0,58484-22-3,70128-27-7,70145-20-9,94482-21-0,98300-76-6
2,3,4,6-tetra-O-acetyl-D-glucosyl-1-amine

: 57620-22-1
N-benzyl-2,4-dinitro-benzenesulfonamide

: 1000278-27-2
N-phenylmethyl-N'-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)butanediamide

Guidance literature:: thiolane-2,5-dione; 2,3,4,6-tetra-O-acetyl-D-glucosyl-1-amine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

N-benzyl-2,4-dinitro-benzenesulfonamide; With caesium carbonate; In N,N-dimethyl-formamide; for 1h; Further stages.;
DOI:10.1021/ol702570x