C₁₇H₁₅I₂NO

Base Information

• Chemical Name: C₁₇H₁₅I₂NO
• CAS No.: 1354310-97-6
• Molecular Formula: C₁₇H₁₅I₂NO
• Molecular Weight: 503.121
• Mol file: 1354310-97-6.mol

Synonyms:C₁₇H₁₅I₂NO

Chemical Property of C₁₇H₁₅I₂NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₅I₂NO

There total 1 articles about C₁₇H₁₅I₂NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 4.0%

C8H9I2N (1354311-18-4) + Cinnamoyl chloride (102-92-1,17082-09-6) → C17H15I2NO (1354310-97-6)

Guidance literature:

C₈H₉I₂N; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.166667h;

Cinnamoyl chloride; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1021/ja211069f

Reference yield: 89.0%

C17H15I2NO (1354310-97-6) + benzyl bromide (100-39-0) → C24H21I2NO

Guidance literature:

With Br^(1-)*C₁₀₂H₁₃₀N⁽¹⁺⁾; potassium hydroxide; In di-isopropyl ether; at -20 ℃; for 30h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;

DOI:10.1021/ja211069f

upstream raw materials:

C₈H₉I₂N

Cinnamoyl chloride