[Cu(acetylacetonato)(1,6-bis(2-chlorophenyl)-2,5-diazahexane)]ClO₄

Base Information

• Chemical Name: [Cu(acetylacetonato)(1,6-bis(2-chlorophenyl)-2,5-diazahexane)]ClO₄
• CAS No.: 872442-06-3
• Molecular Formula: C₅H₇O₂*C₁₆H₁₈Cl₂N₂*ClO₄*Cu
• Molecular Weight: 571.344
• Mol file: 872442-06-3.mol

Synonyms:[Cu(acetylacetonato)(1,6-bis(2-chlorophenyl)-2,5-diazahexane)]ClO₄

Chemical Property of [Cu(acetylacetonato)(1,6-bis(2-chlorophenyl)-2,5-diazahexane)]ClO₄

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [Cu(acetylacetonato)(1,6-bis(2-chlorophenyl)-2,5-diazahexane)]ClO₄

There total 1 articles about [Cu(acetylacetonato)(1,6-bis(2-chlorophenyl)-2,5-diazahexane)]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

copper(II) perchlorate hexahydrate + N1,N2-bis(2-chlorobenzyl)ethane-1,2-diamine (108896-78-2) + acetylacetone (123-54-6,81235-32-7) → [Cu(acetylacetonato)(1,6-bis(2-chlorophenyl)-2,5-diazahexane)]ClO4 (872442-06-3)

Guidance literature:

With Na₂CO₃; In ethanol; water; to a soln. of diamine (5 mml), acetylacetone (5 mmol), Na2CO3 (2.5 mmol)in ethanol were slowly added Cu(ClO4)2*6H2O (5 mmol) in water; the resu lting mixt. was allowed to stand overnight at room temp.; crystals were collected by filtration and washed with hexane; elem. anal.;

DOI:10.1016/j.molstruc.2005.07.018

upstream raw materials:

N¹,N²-bis(2-chlorobenzyl)ethane-1,2-diamine

acetylacetone