2,2-Dimethyl-3-(4-methylsulfanyl-phenyl)-3-oxo-propionic acid methyl ester

Base Information

Chemical Name:2,2-Dimethyl-3-(4-methylsulfanyl-phenyl)-3-oxo-propionic acid methyl ester
CAS No.:108818-70-8
Molecular Formula:C₁₃H₁₆O₃S
Molecular Weight:252.334
Hs Code.:

Synonyms:2,2-Dimethyl-3-(4-methylsulfanyl-phenyl)-3-oxo-propionic acid methyl ester

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Chemical Property of 2,2-Dimethyl-3-(4-methylsulfanyl-phenyl)-3-oxo-propionic acid methyl ester

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Technology Process of 2,2-Dimethyl-3-(4-methylsulfanyl-phenyl)-3-oxo-propionic acid methyl ester

There total 1 articles about 2,2-Dimethyl-3-(4-methylsulfanyl-phenyl)-3-oxo-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108818-59-3
methyl 3-[4-(methylsulfanyl)phenyl]-3-oxopropanoate

: 74-88-4
methyl iodide

: 108818-70-8
2,2-Dimethyl-3-(4-methylsulfanyl-phenyl)-3-oxo-propionic acid methyl ester

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, from 10 to 15 deg C, 2.) DMF, RT, 20 h;
DOI:10.1021/jm00393a007

Reference yield: 62.0%

: 108818-70-8
2,2-Dimethyl-3-(4-methylsulfanyl-phenyl)-3-oxo-propionic acid methyl ester

: 108818-83-3
4,4-Dimethyl-5-(4-methylsulfanyl-phenyl)-2,4-dihydro-pyrazol-3-one

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Heating;
DOI:10.1021/jm00393a007

Reference yield:

: 108818-70-8
2,2-Dimethyl-3-(4-methylsulfanyl-phenyl)-3-oxo-propionic acid methyl ester

: 108818-87-7
2,4-dihydro-5-<4-(methylsulfinyl)phenyl>-4,4-dimethyl-3H-pyrazol-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / 85percent hydrazine hydrate / ethanol / 2 h / Heating

2: 80 percent / mCPBA / CH₂Cl₂ / 0.5 h / Ambient temperature

With hydrazine hydrate; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane;
DOI:10.1021/jm00393a007