[3-(15-bromo-pentadecyloxy)-2-(3,7,11,15-tetramethyl-hexadecyloxy)-propoxymethyl]-benzene

Base Information

Chemical Name:[3-(15-bromo-pentadecyloxy)-2-(3,7,11,15-tetramethyl-hexadecyloxy)-propoxymethyl]-benzene
CAS No.:275820-12-7
Molecular Formula:C₄₅H₈₃BrO₃
Molecular Weight:752.056
Hs Code.:

Synonyms:[3-(15-bromo-pentadecyloxy)-2-(3,7,11,15-tetramethyl-hexadecyloxy)-propoxymethyl]-benzene

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Chemical Property of [3-(15-bromo-pentadecyloxy)-2-(3,7,11,15-tetramethyl-hexadecyloxy)-propoxymethyl]-benzene

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Technology Process of [3-(15-bromo-pentadecyloxy)-2-(3,7,11,15-tetramethyl-hexadecyloxy)-propoxymethyl]-benzene

There total 6 articles about [3-(15-bromo-pentadecyloxy)-2-(3,7,11,15-tetramethyl-hexadecyloxy)-propoxymethyl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 81726-81-0
1,15-dibromopentadecane

: 156473-46-0
3-(benzyloxy)-2-((3,7,11,15-tetramethylhexadecyl)oxy)propan-1-ol

: 275820-12-7
[3-(15-bromo-pentadecyloxy)-2-(3,7,11,15-tetramethyl-hexadecyloxy)-propoxymethyl]-benzene

Guidance literature:: With sodium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)00283-5

Reference yield:

: 275820-16-1
C₃₇H₆₀O₃

: 275820-12-7
[3-(15-bromo-pentadecyloxy)-2-(3,7,11,15-tetramethyl-hexadecyloxy)-propoxymethyl]-benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / H₂ / Pd/C / methanol

2: p-TSA / toluene

3: 69 percent / DIBAL-H / CH₂Cl₂; toluene

4: 52 percent / NaH / tetrahydrofuran

With hydrogen; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; toluene; 1: Catalytic hydrogenation / 2: Condensation / 3: Reduction / 4: Alkylation;
DOI:10.1016/S0040-4039(00)00283-5

Reference yield:

: 106-02-5,81031-90-5
pentadecanolide

: 275820-12-7
[3-(15-bromo-pentadecyloxy)-2-(3,7,11,15-tetramethyl-hexadecyloxy)-propoxymethyl]-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / LiALH₄ / tetrahydrofuran

2: 95 percent / HBr; H₂SO₄

3: 52 percent / NaH / tetrahydrofuran

With lithium aluminium tetrahydride; sulfuric acid; hydrogen bromide; sodium hydride; In tetrahydrofuran; 1: Ring cleavage / 2: Bromination / 3: Alkylation;
DOI:10.1016/S0040-4039(00)00283-5