N,N'-di-p-toluenesulfonyl-N,N'-bis<6-(p-toluenesulfonyloxy)hexyl>-1,6-hexanediamine

Base Information

Chemical Name:N,N'-di-p-toluenesulfonyl-N,N'-bis<6-(p-toluenesulfonyloxy)hexyl>-1,6-hexanediamine
CAS No.:130945-19-6
Molecular Formula:C₄₆H₆₄N₂O₁₀S₄
Molecular Weight:933.286
Hs Code.:

Synonyms:N,N'-di-p-toluenesulfonyl-N,N'-bis<6-(p-toluenesulfonyloxy)hexyl>-1,6-hexanediamine

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Chemical Property of N,N'-di-p-toluenesulfonyl-N,N'-bis<6-(p-toluenesulfonyloxy)hexyl>-1,6-hexanediamine

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Technology Process of N,N'-di-p-toluenesulfonyl-N,N'-bis<6-(p-toluenesulfonyloxy)hexyl>-1,6-hexanediamine

There total 8 articles about N,N'-di-p-toluenesulfonyl-N,N'-bis<6-(p-toluenesulfonyloxy)hexyl>-1,6-hexanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 130945-15-2
N,N'-bis(6-hydroxyhexyl)-N,N'-di-p-toluenesulfonyl-1,6-hexanediamine

: 104-15-4
toluene-4-sulfonic acid

: 130945-19-6
N,N'-di-p-toluenesulfonyl-N,N'-bis<6-(p-toluenesulfonyloxy)hexyl>-1,6-hexanediamine

Guidance literature:: With N,N'-dimethylaminopyridine; triethylamine; In dichloromethane; for 3h; Ambient temperature;

Reference yield:

: 124-09-4
1,6-Hexanediamine

: 130945-19-6
N,N'-di-p-toluenesulfonyl-N,N'-bis<6-(p-toluenesulfonyloxy)hexyl>-1,6-hexanediamine

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / triethylamine, N,N'-dimethylaminopyridine / CH₂Cl₂ / 3 h / Ambient temperature

2: 1.) NaH / 1.) DMF, 60 deg C, 20 to 25 mm Hg, 30 min 2.) DMF, 60 deg C, 3 h

3: 94 percent / p-toluenesulfonic acid / methanol / 0.5 h / Ambient temperature

4: 96 percent / triethylamine, N,N'-dimethylaminopyridine / CH₂Cl₂ / 3 h / Ambient temperature

With N,N'-dimethylaminopyridine; sodium hydride; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane;

Reference yield:

: 53963-10-3
2-[(6-bromohexyl)oxy]tetrahydro-2H-pyran

: 130945-19-6
N,N'-di-p-toluenesulfonyl-N,N'-bis<6-(p-toluenesulfonyloxy)hexyl>-1,6-hexanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 60 deg C, 20 to 25 mm Hg, 30 min 2.) DMF, 60 deg C, 3 h

2: 94 percent / p-toluenesulfonic acid / methanol / 0.5 h / Ambient temperature

3: 96 percent / triethylamine, N,N'-dimethylaminopyridine / CH₂Cl₂ / 3 h / Ambient temperature

With N,N'-dimethylaminopyridine; sodium hydride; toluene-4-sulfonic acid; triethylamine; In methanol; dichloromethane;