(4R,5R)-4,5-Bis((2-methylethoxy)carbonyl)-2-(trans-2-phenylethenyl)-1,3-dioxolane

Base Information

Chemical Name:(4R,5R)-4,5-Bis((2-methylethoxy)carbonyl)-2-(trans-2-phenylethenyl)-1,3-dioxolane
CAS No.:99267-72-8
Molecular Formula:C₁₉H₂₄O₆
Molecular Weight:348.396
Hs Code.:

Synonyms:(4R,5R)-4,5-Bis((2-methylethoxy)carbonyl)-2-(trans-2-phenylethenyl)-1,3-dioxolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5R)-4,5-Bis((2-methylethoxy)carbonyl)-2-(trans-2-phenylethenyl)-1,3-dioxolane

Chemical Property:

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Technology Process of (4R,5R)-4,5-Bis((2-methylethoxy)carbonyl)-2-(trans-2-phenylethenyl)-1,3-dioxolane

There total 3 articles about (4R,5R)-4,5-Bis((2-methylethoxy)carbonyl)-2-(trans-2-phenylethenyl)-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2217-15-4
L-(+)-diisopropyl tartrate

: 25226-98-6
trans-cinnamaldehyde diethylacetal

: 99267-72-8
(4R,5R)-4,5-Bis((2-methylethoxy)carbonyl)-2-(trans-2-phenylethenyl)-1,3-dioxolane

Guidance literature:: With pyridinium p-toluenesulfonate; In benzene; for 1h; Heating;
DOI:10.1016/S0040-4020(01)88107-2

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 99267-72-8
(4R,5R)-4,5-Bis((2-methylethoxy)carbonyl)-2-(trans-2-phenylethenyl)-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium nitrate / ethanol / Ambient temperature

2: 93 percent / pyridinium tosylate / benzene / 1 h / Heating

With pyridinium p-toluenesulfonate; ammonium nitrate; In ethanol; benzene;
DOI:10.1016/S0040-4020(01)88107-2

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 2217-15-4
L-(+)-diisopropyl tartrate

: 99267-72-8
(4R,5R)-4,5-Bis((2-methylethoxy)carbonyl)-2-(trans-2-phenylethenyl)-1,3-dioxolane

Guidance literature:: With ammonium nitrate; toluene-4-sulfonic acid; orthoformic acid triethyl ester; Yield given. Multistep reaction; 1.) EtOH, 25 deg C, 2.) C₆H₆, 80 deg C;
DOI:10.1039/c39940001783