3-methyl-5-(2,2,6-trimethyl-cyclohex-5-enylidene)-pent-3-enoic acid-ethyl ester

Base Information

• Chemical Name: 3-methyl-5-(2,2,6-trimethyl-cyclohex-5-enylidene)-pent-3-enoic acid-ethyl ester
• CAS No.: 94802-08-1
• Molecular Formula: C₁₇H₂₆O₂
• Molecular Weight: 262.392

Synonyms:3-methyl-5-(2,2,6-trimethyl-cyclohex-5-enylidene)-pent-3-enoic acid-ethyl ester

Chemical Property of 3-methyl-5-(2,2,6-trimethyl-cyclohex-5-enylidene)-pent-3-enoic acid-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-methyl-5-(2,2,6-trimethyl-cyclohex-5-enylidene)-pent-3-enoic acid-ethyl ester

There total 2 articles about 3-methyl-5-(2,2,6-trimethyl-cyclohex-5-enylidene)-pent-3-enoic acid-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-β-ionone (79-77-6,14901-07-6) + ethyl bromoacetate (105-36-2) → (2E,4E)-ethyl 3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2,4-dienoate (17974-55-9) + 3-methyl-5-(2,2,6-trimethyl-cyclohex-5-enylidene)-pent-3-enoic acid-ethyl ester (94802-08-1)

Guidance literature:

With zinc; benzene; anschliessendes Behandeln mit wss. Essigsaeure und Erhitzen mit Kaliumhydrogensulfat auf 150grad;

DOI:10.1021/ja01200a519 DOI:10.1021/ja01232a005

Reference yield:

→ 3-methyl-5-(2,2,6-trimethyl-cyclohex-5-enylidene)-pent-3-enoic acid-ethyl ester (94802-08-1)

Guidance literature:

β-Ionon, 1.) Ae., Ethoxy-ethinyl-magnesiumbromid in Ae., N2, -10grad bis -12grad (-> rotes Oel), 2.) 10percentig. H2SO4;

Reference yield:

3-methyl-5-(2,2,6-trimethyl-cyclohex-5-enylidene)-pent-3-enoic acid-ethyl ester (94802-08-1) → 3-methyl-5-(2,6,6-trimethyl-cyclohex-2-enylidene)-pent-3-en-1-ol

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

upstream raw materials:

(E)-β-ionone

ethyl bromoacetate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 94802-08-1 3-methyl-5-(2,2,6-trimethyl-cyclohex-5-enylidene)-pent-3-enoic acid-ethyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send