tert-butyl 3-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)-6-benzyloxyhexanoate

Base Information

Chemical Name:tert-butyl 3-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)-6-benzyloxyhexanoate
CAS No.:1404379-05-0
Molecular Formula:C₂₈H₃₅NO₆
Molecular Weight:481.589
Hs Code.:

Synonyms:tert-butyl 3-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)-6-benzyloxyhexanoate

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Chemical Property of tert-butyl 3-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)-6-benzyloxyhexanoate

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Technology Process of tert-butyl 3-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)-6-benzyloxyhexanoate

There total 4 articles about tert-butyl 3-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)-6-benzyloxyhexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 253882-47-2
(R)-4-benzyl-3-(5-benzyloxy-pentanoyl)oxazolidin-2-one

: 1404379-05-0
tert-butyl 3-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)-6-benzyloxyhexanoate

Guidance literature:: (R)-4-benzyl-3-(5-benzyloxy-pentanoyl)oxazolidin-2-one; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - -40 ℃;

bromoacetic acid tert-butyl ester; In tetrahydrofuran; at -78 - -36 ℃;

With N,N,N'-triethylethanediamine; In tetrahydrofuran; Cooling with ice;

Reference yield:

: 100-39-0
benzyl bromide

: 1404379-05-0
tert-butyl 3-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)-6-benzyloxyhexanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / toluene / 125 °C

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / chloroform / 2.5 h / 20 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 - -40 °C

3.2: -78 - -36 °C

3.3: Cooling with ice

With dmap; sodium hexamethyldisilazane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In tetrahydrofuran; chloroform; toluene;

Reference yield:

: 542-28-9,26354-94-9
3,4,5,6-tetrahydro-2H-pyran-2-one

: 1404379-05-0
tert-butyl 3-((R)-4-benzyl-2-oxooxazolidine-3-carbonyl)-6-benzyloxyhexanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium hydroxide / toluene / 125 °C

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / chloroform / 2.5 h / 20 °C

3.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 - -40 °C

3.2: -78 - -36 °C

3.3: Cooling with ice

With dmap; sodium hexamethyldisilazane; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In tetrahydrofuran; chloroform; toluene;