di(1-oxoperhydro-1λ⁵-[1,3,2]diazaphospholo[1,5-a]pyridin-1-yl) (4-bromophenyl)boronate

Base Information

• Chemical Name: di(1-oxoperhydro-1λ⁵-[1,3,2]diazaphospholo[1,5-a]pyridin-1-yl) (4-bromophenyl)boronate
• CAS No.: 1374987-91-3
• Molecular Formula: C₁₈H₂₈BBrN₄O₄P₂
• Molecular Weight: 517.107

Synonyms:di(1-oxoperhydro-1λ⁵-[1,3,2]diazaphospholo[1,5-a]pyridin-1-yl) (4-bromophenyl)boronate

Chemical Property of di(1-oxoperhydro-1λ⁵-[1,3,2]diazaphospholo[1,5-a]pyridin-1-yl) (4-bromophenyl)boronate

Chemical Property:

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Technology Process of di(1-oxoperhydro-1λ⁵-[1,3,2]diazaphospholo[1,5-a]pyridin-1-yl) (4-bromophenyl)boronate

There total 2 articles about di(1-oxoperhydro-1λ⁵-[1,3,2]diazaphospholo[1,5-a]pyridin-1-yl) (4-bromophenyl)boronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1-chlorooctahydro-1λ5-[1,3,2]diazaphospholo[1,5-a]pyridine-1-oxide (1353131-54-0) + 4-Bromophenylboronic acid (5467-74-3) → di(1-oxoperhydro-1λ5-[1,3,2]diazaphospholo[1,5-a]pyridin-1-yl) (4-bromophenyl)boronate (1374987-91-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 45 ℃;

DOI:10.1002/hc.21010

Reference yield:

C-piperidin-2-yl-methylamine (22990-77-8,111478-74-1,111478-77-4) → di(1-oxoperhydro-1λ5-[1,3,2]diazaphospholo[1,5-a]pyridin-1-yl) (4-bromophenyl)boronate (1374987-91-3)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine; trichlorophosphate / tetrahydrofuran / 0 - 20 °C

2: triethylamine / tetrahydrofuran / 0 - 45 °C

With triethylamine; trichlorophosphate; In tetrahydrofuran;

DOI:10.1002/hc.21010

upstream raw materials:

C-piperidin-2-yl-methylamine

1-chlorooctahydro-1λ⁵-[1,3,2]diazaphospholo[1,5-a]pyridine-1-oxide

4-Bromophenylboronic acid

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