bis(cyclohexenyl)-N-methyl-N-phenylboranamine

Base Information

Chemical Name:bis(cyclohexenyl)-N-methyl-N-phenylboranamine
CAS No.:83720-54-1
Molecular Formula:C₁₉H₂₆BN
Molecular Weight:279.233
Hs Code.:

Synonyms:bis(cyclohexenyl)-N-methyl-N-phenylboranamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(cyclohexenyl)-N-methyl-N-phenylboranamine

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Technology Process of bis(cyclohexenyl)-N-methyl-N-phenylboranamine

There total 1 articles about bis(cyclohexenyl)-N-methyl-N-phenylboranamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1125-73-1
N-methylanilinoborane dichloride

: 37609-34-0
cyclohex-1-en-1-yllithium

: 83720-54-1
bis(cyclohexenyl)-N-methyl-N-phenylboranamine

Guidance literature:: In diethyl ether; soln. of B compd. in Et2O immersed in ice bath, soln. of org. compd. inEt2O added during a period of ca. 5 min, mixture stirred at room temp. for 3 h; filtration under N2, evapn. in vac., distn.; elem. anal.;
DOI:10.1021/ja00390a024

Reference yield: 80.0%

: 83720-54-1
bis(cyclohexenyl)-N-methyl-N-phenylboranamine

: 83720-63-2
10-(1-cyclohexenyl)-9-methyl-1,2,3,4,4a,9,10,10a-octahydro-9-aza-10-boraphenanthrene

Guidance literature:: In cyclohexane; Irradiation (UV/VIS); B compd. in cyclohexane irradiated with medium-pressure mercury lamp under N2 for 50 h; evapn. in vac., distn.;
DOI:10.1021/ja00390a024

Reference yield:

: 83720-54-1
bis(cyclohexenyl)-N-methyl-N-phenylboranamine

: 83721-11-3
10-(1-cyclohexenyl)-9-methyl-1,2,3,4,4a,9,10,10a-octahydro-9-aza-10-boraphenanthrene

Guidance literature:: In cyclohexane; Irradiation (UV/VIS); soln. of B compd. in cyclohexane irradiated with medium-pressure mercury lamp for 50 h under N2; evapn. in vac., distn.in vac.; elem. anal.;
DOI:10.1021/ja00390a025