C₁₂H₁₂N₄OS

Base Information

Chemical Name:C₁₂H₁₂N₄OS
CAS No.:1263144-11-1
Molecular Formula:C₁₂H₁₂N₄OS
Molecular Weight:260.319
Hs Code.:

C<sub>12</sub>H<sub>12</sub>N<sub>4</sub>OS

Synonyms:C₁₂H₁₂N₄OS

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Chemical Property of C₁₂H₁₂N₄OS

Chemical Property:

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Technology Process of C₁₂H₁₂N₄OS

There total 1 articles about C₁₂H₁₂N₄OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1150307-99-5
5-(but-3-yn-1-ylthio)-1-phenyl-1H-tetrazole

: 1263144-11-1
C₁₂H₁₂N₄OS

Guidance literature:: 5-(but-3-yn-1-ylthio)-1-phenyl-1H-tetrazole; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.75h;

formaldehyd; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.5h;

With ammonium chloride; In water; at 20 ℃;
DOI:10.1016/j.tet.2010.11.017

Reference yield: 100.0%

: 1263144-11-1
C₁₂H₁₂N₄OS

: 1263144-27-9
C₁₂H₁₂N₄O₃S

Guidance literature:: With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In ethanol; water; at 20 ℃; for 31h;
DOI:10.1016/j.tet.2010.11.017

Reference yield:

: 1263144-11-1
C₁₂H₁₂N₄OS

: C₃₂H₄₈O₆Si

: 1263144-07-5
C₃₂H₄₈O₆Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide / ethanol; water / 31 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 7 h / 20 °C

3.1: potassium hexamethylsilazane / 1,2-dimethoxyethane / 0.5 h / -75 - -65 °C

3.2: 3 h / -75 - 0 °C

With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine; In 1,2-dimethoxyethane; ethanol; water; 1,2-dichloro-ethane; 3.1: Julia-Kocienski reaction / 3.2: Julia-Kocienski reaction;
DOI:10.1016/j.tet.2010.11.017