C₃₀H₂₇ClN₂O₅

Base Information

Chemical Name:C₃₀H₂₇ClN₂O₅
CAS No.:1423689-66-0
Molecular Formula:C₃₀H₂₇ClN₂O₅
Molecular Weight:531.008
Hs Code.:

C<sub>30</sub>H<sub>27</sub>ClN<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₀H₂₇ClN₂O₅

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Chemical Property of C₃₀H₂₇ClN₂O₅

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Technology Process of C₃₀H₂₇ClN₂O₅

There total 12 articles about C₃₀H₂₇ClN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1265631-09-1
[3-(4-bromo-phenyl)-5-methyl-isoxazol-4-yl]-carbamic acid (R)-1-(2-chloro-phenyl)-ethyl ester

: 1396007-85-4
1-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-cyclopropanecarboxylic acid methyl ester

: 1423689-66-0
C₃₀H₂₇ClN₂O₅

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In 1,2-dimethoxyethane; water; at 90 ℃; Inert atmosphere;

Reference yield:

: 2142-68-9
1-(2-chlorophenyl)ethanone

: 1423689-66-0
C₃₀H₂₇ClN₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1: (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / 0.5 h / 20 °C

2: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 80 °C

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 90 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; dimethylsulfide borane complex; diphenyl phosphoryl azide; sodium carbonate; triethylamine; (S)-tetrahydro-1-butyl-3,3-diphenyl-1H,3H-pyrrolo{2,1-c}{1,3,2}oxazaborole; In tetrahydrofuran; 1,2-dimethoxyethane; water; toluene;

Reference yield:

: 25062-46-8,40979-16-6,34158-73-1
4-bromobenzaldehyde oxime

: 1423689-66-0
C₃₀H₂₇ClN₂O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 2 h / 15 - 20 °C

2.1: sodium methylate / methanol / 0.67 h / 0 - 25 °C

3.1: water; sodium hydroxide / tetrahydrofuran / 3 h / 20 °C

3.2: pH Ca_. 3 / Cooling with ice

4.1: diphenyl phosphoryl azide; triethylamine / toluene / 3 h / 80 °C

5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 90 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-chloro-succinimide; diphenyl phosphoryl azide; water; sodium methylate; sodium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; toluene;