5-[1-(4-Fluoro-phenyl)-meth-(E)-ylidene]-1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octan-6-one oxime

Base Information

Chemical Name:5-[1-(4-Fluoro-phenyl)-meth-(E)-ylidene]-1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octan-6-one oxime
CAS No.:135488-34-5
Molecular Formula:C₁₇H₂₀FNO₂
Molecular Weight:289.35
Hs Code.:

Synonyms:5-[1-(4-Fluoro-phenyl)-meth-(E)-ylidene]-1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octan-6-one oxime

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Chemical Property of 5-[1-(4-Fluoro-phenyl)-meth-(E)-ylidene]-1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octan-6-one oxime

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Technology Process of 5-[1-(4-Fluoro-phenyl)-meth-(E)-ylidene]-1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octan-6-one oxime

There total 1 articles about 5-[1-(4-Fluoro-phenyl)-meth-(E)-ylidene]-1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octan-6-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 135488-37-8
5-[1-(4-Fluoro-phenyl)-meth-(E)-ylidene]-1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octan-6-one

: 135488-34-5
5-[1-(4-Fluoro-phenyl)-meth-(E)-ylidene]-1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octan-6-one oxime

Guidance literature:: With hydroxylamine hydrochloride; In pyridine; ethanol; for 14h; Heating;

Reference yield:

: 1458-63-5
N-(3-chloropropyl)-piperidine

: 135488-34-5
5-[1-(4-Fluoro-phenyl)-meth-(E)-ylidene]-1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octan-6-one oxime

: 135488-26-5
5-[1-(4-Fluoro-phenyl)-meth-(E)-ylidene]-1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octan-6-one O-(3-piperidin-1-yl-propyl)-oxime

Guidance literature:: With sodium methylate; Yield given. Multistep reaction; 1) CH₃OH, reflux, 30 min., 2) DMF, a) 50 deg C, 3h, b) RT, 12 h;

Reference yield:

: 3240-94-6
N-(2-chlorethyl)morpholine

: 135488-34-5
5-[1-(4-Fluoro-phenyl)-meth-(E)-ylidene]-1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octan-6-one oxime

: 135488-24-3
5-[1-(4-Fluoro-phenyl)-meth-(E)-ylidene]-1,3,3-trimethyl-2-oxa-bicyclo[2.2.2]octan-6-one O-(2-morpholin-4-yl-ethyl)-oxime

Guidance literature:: With sodium methylate; Yield given. Multistep reaction; 1) CH₃OH, reflux, 30 min., 2) DMF, a) 50 deg C, 3h, b) RT, 12 h;