(R)-N-(4-hydroxy-2-methylbutyl)-4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide

Base Information

Chemical Name:(R)-N-(4-hydroxy-2-methylbutyl)-4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide
CAS No.:1443054-45-2
Molecular Formula:C₁₇H₂₇NO₃S
Molecular Weight:325.472
Hs Code.:

Synonyms:(R)-N-(4-hydroxy-2-methylbutyl)-4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide

Suppliers and Price of (R)-N-(4-hydroxy-2-methylbutyl)-4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-N-(4-hydroxy-2-methylbutyl)-4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide

Chemical Property:

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Technology Process of (R)-N-(4-hydroxy-2-methylbutyl)-4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide

There total 5 articles about (R)-N-(4-hydroxy-2-methylbutyl)-4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1443054-46-3
C₃₃H₄₅NO₃SSi

: 1443054-45-2
(R)-N-(4-hydroxy-2-methylbutyl)-4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 3h;
DOI:10.1021/ja4047312

Reference yield:

: 78388-19-9
4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide

: 1443054-45-2
(R)-N-(4-hydroxy-2-methylbutyl)-4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 1 h

1.2: 18 h

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja4047312

Reference yield:

: 213740-15-9
(2R)-4-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-2-methylbutan-1-ol

: 1443054-45-2
(R)-N-(4-hydroxy-2-methylbutyl)-4-methyl-N-(3-methylbut-2-enyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole; triphenylphosphine; iodine / chloroform / 18 h

2.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 1 h

2.2: 18 h

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h

With 1H-imidazole; tetrabutyl ammonium fluoride; iodine; sodium hydride; triphenylphosphine; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ja4047312