Ir(CH₃C₂CH₃)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*BF₄^(1-)={Ir(CH₃C₂CH₃)(P(CH₃)2C₆H₅)3}BF₄

Base Information

• Chemical Name: Ir(CH₃C₂CH₃)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*BF₄^(1-)={Ir(CH₃C₂CH₃)(P(CH₃)2C₆H₅)3}BF₄
• CAS No.: 119680-94-3
• Molecular Formula: BF₄*C₂₈H₃₉IrP₃
• Molecular Weight: 747.564

Synonyms:Ir(CH₃C₂CH₃)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*BF₄^(1-)={Ir(CH₃C₂CH₃)(P(CH₃)2C₆H₅)3}BF₄

Chemical Property of Ir(CH₃C₂CH₃)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*BF₄^(1-)={Ir(CH₃C₂CH₃)(P(CH₃)2C₆H₅)3}BF₄

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Technology Process of Ir(CH₃C₂CH₃)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*BF₄^(1-)={Ir(CH₃C₂CH₃)(P(CH₃)2C₆H₅)3}BF₄

There total 1 articles about Ir(CH₃C₂CH₃)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*BF₄^(1-)={Ir(CH₃C₂CH₃)(P(CH₃)2C₆H₅)3}BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

dimethylacetylene (503-17-3) + {Ir(η2-H2)H2(PMe2Ph)3}BF4 (115983-32-9) → Ir(CH3C2CH3)(P(CH3)2C6H5)3(1+)*BF4(1-)={Ir(CH3C2CH3)(P(CH3)2C6H5)3}BF4 (119680-94-3)

Guidance literature:

In dichloromethane; byproducts: cis-2-butene, 1-butene; 5 equivs. of 2-butyne per Ir complex; elem. anal.;

DOI:10.1021/ja00188a083

Reference yield:

Ir(CH3C2CH3)(P(CH3)2C6H5)3(1+)*BF4(1-)={Ir(CH3C2CH3)(P(CH3)2C6H5)3}BF4 (119680-94-3) + dimethyl acetylenedicarboxylate (762-42-5) → {Ir(P(CH3)2C6H5)3(CH3O2CC2CO2CH3)2}(1+)*BF4(1-)={Ir(P(CH3)2C6H5)3(CH3O2CC2CO2CH3)2}BF4 (131006-87-6)

Guidance literature:

In dichloromethane; dissolving the Ir(I) complex salt in CH2Cl2 under N2, addn. of the acetylenedicarboxylate via syringe, stirring (10 h), removing solvent and excess acetylenedicarboxylate (vac.) to give a red oil;

DOI:10.1016/S0277-5387(00)83999-6

upstream raw materials:

dimethylacetylene

{Ir(η2-H2)H2(PMe2Ph)3}BF4

Downstream raw materials:

{Ir(P(CH₃)2C₆H₅)3(CH₃O₂CC₂CO₂CH₃)2}⁽¹⁺⁾*BF₄^(1-)={Ir(P(CH₃)2C₆H₅)3(CH₃O₂CC₂CO₂CH₃)2}BF₄

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