(1S^*,2S^*,7aR^*,7bR^*)-1-pyrrolidinocarbonyl-2-benzoyloxymethyl-5,6-methylenedioxy-8,9,10-trimethoxy-1,2,3,12-tetrahydrobenzo<4.5:6.7>cyclooctene

Base Information

• Chemical Name: (1S^*,2S^*,7aR^*,7bR^*)-1-pyrrolidinocarbonyl-2-benzoyloxymethyl-5,6-methylenedioxy-8,9,10-trimethoxy-1,2,3,12-tetrahydrobenzo<4.5:6.7>cyclooctene
• CAS No.: 96960-68-8
• Molecular Formula: C₃₃H₃₅NO₈
• Molecular Weight: 573.643

Synonyms:(1S^*,2S^*,7aR^*,7bR^*)-1-pyrrolidinocarbonyl-2-benzoyloxymethyl-5,6-methylenedioxy-8,9,10-trimethoxy-1,2,3,12-tetrahydrobenzo<4.5:6.7>cyclooctene

Chemical Property of (1S^*,2S^*,7aR^*,7bR^*)-1-pyrrolidinocarbonyl-2-benzoyloxymethyl-5,6-methylenedioxy-8,9,10-trimethoxy-1,2,3,12-tetrahydrobenzo<4.5:6.7>cyclooctene

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Technology Process of (1S^*,2S^*,7aR^*,7bR^*)-1-pyrrolidinocarbonyl-2-benzoyloxymethyl-5,6-methylenedioxy-8,9,10-trimethoxy-1,2,3,12-tetrahydrobenzo<4.5:6.7>cyclooctene

There total 2 articles about (1S^*,2S^*,7aR^*,7bR^*)-1-pyrrolidinocarbonyl-2-benzoyloxymethyl-5,6-methylenedioxy-8,9,10-trimethoxy-1,2,3,12-tetrahydrobenzo<4.5:6.7>cyclooctene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

benzoyl chloride (98-88-4) + C26H31NO7 (96960-67-7) → (1S*,2S*,7aR*,7bR*)-1-pyrrolidinocarbonyl-2-benzoyloxymethyl-5,6-methylenedioxy-8,9,10-trimethoxy-1,2,3,12-tetrahydrobenzo<4.5:6.7>cyclooctene (96960-68-8)

Guidance literature:

With triethylamine; In dichloromethane; for 20h; Ambient temperature;

DOI:10.1248/cpb.33.609

Reference yield:

(+/-)-isostegane (61038-90-2,70051-17-1,70051-18-2,72258-40-3,72258-54-9,72657-29-5,72657-64-8,76250-31-2,92283-76-6,92283-77-7,96744-76-2,96744-77-3,96744-78-4,96744-79-5) → (1S*,2S*,7aR*,7bR*)-1-pyrrolidinocarbonyl-2-benzoyloxymethyl-5,6-methylenedioxy-8,9,10-trimethoxy-1,2,3,12-tetrahydrobenzo<4.5:6.7>cyclooctene (96960-68-8)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 48 h / Ambient temperature

2: 79 percent / NEt₃ / CH₂Cl₂ / 20 h / Ambient temperature

With triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1248/cpb.33.609

upstream raw materials:

benzoyl chloride

C₂₆H₃₁NO₇

(+/-)-isostegane

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