d-3-phenylpropiolic acid

Base Information

• Chemical Name: d-3-phenylpropiolic acid
• CAS No.: 1033320-59-0
• Molecular Formula: C₉H₆O₂
• Molecular Weight: 147.137
• Mol file: 1033320-59-0.mol

Synonyms:d-3-phenylpropiolic acid

Chemical Property of d-3-phenylpropiolic acid

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of d-3-phenylpropiolic acid

There total 1 articles about d-3-phenylpropiolic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

phenylpropyolic acid (637-44-5) → d-3-phenylpropiolic acid (1033320-59-0)

Guidance literature:

With water-d2; at 20 ℃; for 0.5h;

DOI:10.1002/chem.200701245

Reference yield: 96.0%

d-3-phenylpropiolic acid (1033320-59-0) → C9H5(2)H5O2 (634897-86-2)

Guidance literature:

With 10% Pd/C; hydrogen; water-d2; In methanol; at 20 ℃; for 11h; chemoselective reaction;

DOI:10.1002/chem.200701245

Reference yield: 92.0%

d-3-phenylpropiolic acid (1033320-59-0) + (1-fluoro-2,2-diiodovinyl)benzene → (Z)-(1-fluorobut-1-en-3-yne-1,4-diyl)dibenzene

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,4-di(diphenylphosphino)-butane; In dimethyl sulfoxide; at 100 ℃; Sealed tube;

DOI:10.1021/acs.orglett.9b02907

upstream raw materials:

phenylpropyolic acid

Downstream raw materials:

C₉H₅⁽²⁾H₅O₂