tetra-tert-butyl N-(4-nitrobenzoyl)-γ-L-glutamyl-γ-L-glutamyl-L-glutamate

Base Information

Chemical Name:tetra-tert-butyl N-(4-nitrobenzoyl)-γ-L-glutamyl-γ-L-glutamyl-L-glutamate
CAS No.:133042-44-1
Molecular Formula:C₃₈H₅₈N₄O₁₃
Molecular Weight:778.898
Hs Code.:

Synonyms:tetra-tert-butyl N-(4-nitrobenzoyl)-γ-L-glutamyl-γ-L-glutamyl-L-glutamate

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Chemical Property of tetra-tert-butyl N-(4-nitrobenzoyl)-γ-L-glutamyl-γ-L-glutamyl-L-glutamate

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Technology Process of tetra-tert-butyl N-(4-nitrobenzoyl)-γ-L-glutamyl-γ-L-glutamyl-L-glutamate

There total 1 articles about tetra-tert-butyl N-(4-nitrobenzoyl)-γ-L-glutamyl-γ-L-glutamyl-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 122-04-3
4-nitro-benzoyl chloride

: tetra-tert-butyl γ-L-glutamyl-γ-L-glutamyl-L-glutamate

: 133042-44-1
tetra-tert-butyl N-(4-nitrobenzoyl)-γ-L-glutamyl-γ-L-glutamyl-L-glutamate

Guidance literature:: With 4-methyl-morpholine; In dichloromethane; at 25 ℃; for 1.5h;
DOI:10.1021/jo00010a038

Reference yield: 52.0%

: 133042-44-1
tetra-tert-butyl N-(4-nitrobenzoyl)-γ-L-glutamyl-γ-L-glutamyl-L-glutamate

: 117559-42-9
tetra-tert-butyl N-(4-aminobenzoyl)-γ-L-glutamyl-γ-L-glutamyl-L-glutamate

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethanol; acetic acid; for 2h; under 2482.3 Torr;
DOI:10.1021/jo00010a038

Reference yield:

: 133042-44-1
tetra-tert-butyl N-(4-nitrobenzoyl)-γ-L-glutamyl-γ-L-glutamyl-L-glutamate

: 133042-51-0
tetra-tert-butyl <4-amino>benzoyl>-γ-L-glutamyl-γ-L-glutamyl-L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / H₂ / PtO₂ / ethanol; acetic acid / 2 h / 2482.3 Torr

2: 19 percent / diisopropylethylamine / acetonitrile / 42 h / Ambient temperature

With hydrogen; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; In ethanol; acetic acid; acetonitrile;
DOI:10.1021/jo00010a038