(R)-phenyl-o-anisylphenylphosphinite

Base Information

Chemical Name:(R)-phenyl-o-anisylphenylphosphinite
CAS No.:1417912-03-8
Molecular Formula:C₁₉H₁₇O₂P
Molecular Weight:308.317
Hs Code.:

Synonyms:(R)-phenyl-o-anisylphenylphosphinite

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Chemical Property of (R)-phenyl-o-anisylphenylphosphinite

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Technology Process of (R)-phenyl-o-anisylphenylphosphinite

There total 6 articles about (R)-phenyl-o-anisylphenylphosphinite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: (R)-phenyl-o-anisylphenylphosphinite-borane

: 1417912-03-8
(R)-phenyl-o-anisylphenylphosphinite

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In toluene; at 20 ℃; stereoselective reaction; Inert atmosphere;
DOI:10.1021/acs.orglett.6b01275

Reference yield:

: (2S_P,4R,5S)-(-)-3,4-dimethyl-2,5-diphenyl-1,3,2-oxazaphospholidine borane

: 1417912-03-8
(R)-phenyl-o-anisylphenylphosphinite

Guidance literature:: Multi-step reaction with 4 steps

1: Inert atmosphere

2: toluene / 1 h / 20 °C / Inert atmosphere

3: tetrahydrofuran; toluene / -78 - 20 °C / Inert atmosphere

4: 1,4-diaza-bicyclo[2.2.2]octane / toluene / 20 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; In tetrahydrofuran; toluene;
DOI:10.1021/acs.orglett.6b01275

Reference yield:

: 31600-86-9
2-methoxyphenyllithium

: 1417912-03-8
(R)-phenyl-o-anisylphenylphosphinite

Guidance literature:: Multi-step reaction with 4 steps

1: Inert atmosphere

2: toluene / 1 h / 20 °C / Inert atmosphere

3: tetrahydrofuran; toluene / -78 - 20 °C / Inert atmosphere

4: 1,4-diaza-bicyclo[2.2.2]octane / toluene / 20 °C / Inert atmosphere

With 1,4-diaza-bicyclo[2.2.2]octane; In tetrahydrofuran; toluene;
DOI:10.1021/acs.orglett.6b01275