4-phenyl-2,3-phenantrenedicarboxylic acid anhydride

Base Information

Chemical Name:4-phenyl-2,3-phenantrenedicarboxylic acid anhydride
CAS No.:114468-92-7
Molecular Formula:C₂₂H₁₂O₃
Molecular Weight:324.335
Hs Code.:

Synonyms:4-phenyl-2,3-phenantrenedicarboxylic acid anhydride

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Chemical Property of 4-phenyl-2,3-phenantrenedicarboxylic acid anhydride

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Technology Process of 4-phenyl-2,3-phenantrenedicarboxylic acid anhydride

There total 5 articles about 4-phenyl-2,3-phenantrenedicarboxylic acid anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 108-31-6
maleic anhydride

: 4919-69-1
(2-methylnaphthalen-1-yl)(phenyl)methanone

: 114468-92-7
4-phenyl-2,3-phenantrenedicarboxylic acid anhydride

Guidance literature:: (2-methylnaphthalen-1-yl)(phenyl)methanone; With bromine; In tetrachloromethane; Irradiation;

maleic anhydride; In tetrachloromethane; chloroform; Heating;
DOI:10.1007/s11176-005-0320-0

Reference yield:

: 76635-70-6
(1-bromo-2-naphthyl)methanol

: 114468-92-7
4-phenyl-2,3-phenantrenedicarboxylic acid anhydride

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) TsOH, 2.) conc. HCl / 1.) toluene, reflux, 14 h, 2.) reflux, 1 h

With hydrogenchloride; toluene-4-sulfonic acid;
DOI:10.1021/jo00248a009

Reference yield:

: 114468-87-0
1-amino-1,3-dihydro-1-phenylnaphto<1,2-c>furan

: 110-16-7,26099-09-2
maleic acid

: 114468-92-7
4-phenyl-2,3-phenantrenedicarboxylic acid anhydride

Guidance literature:: With hydrogenchloride; toluene-4-sulfonic acid; Yield given. Multistep reaction; 1.) toluene, reflux, 14 h, 2.) reflux, 1 h;
DOI:10.1021/jo00248a009