2-[4-ethyl-5-(4-methoxyphenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-1-phenyl-ethanone

Base Information

Chemical Name:2-[4-ethyl-5-(4-methoxyphenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-1-phenyl-ethanone
CAS No.:485342-68-5
Molecular Formula:C₁₉H₁₉N₃O₂S
Molecular Weight:353.445
Hs Code.:

Synonyms:2-[4-ethyl-5-(4-methoxyphenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-1-phenyl-ethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[4-ethyl-5-(4-methoxyphenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-1-phenyl-ethanone

Chemical Property:

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Technology Process of 2-[4-ethyl-5-(4-methoxyphenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-1-phenyl-ethanone

There total 5 articles about 2-[4-ethyl-5-(4-methoxyphenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-1-phenyl-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 4-ethyl-5-(4-methoxy-phenyl)-4H-[1,2,4]triazole-3-thiol

: 70-11-1
α-bromoacetophenone

: 485342-68-5
2-[4-ethyl-5-(4-methoxyphenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-1-phenyl-ethanone

Guidance literature:: With triethylamine; In acetonitrile; Reflux;
DOI:10.1016/j.bmc.2013.04.022

Reference yield:

: 3290-99-1
4-methoxybenzoic acid hydrazide

: 485342-68-5
2-[4-ethyl-5-(4-methoxyphenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-1-phenyl-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol

2: sodium hydroxide

3: triethylamine / acetonitrile / Reflux

With triethylamine; sodium hydroxide; In ethanol; acetonitrile;
DOI:10.1016/j.bmc.2013.04.022

Reference yield:

: 100-09-4
4-methoxybenzoic acid

: 485342-68-5
2-[4-ethyl-5-(4-methoxyphenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-1-phenyl-ethanone

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid

2: hydrazine hydrate / ethanol

3: ethanol

4: sodium hydroxide

5: triethylamine / acetonitrile / Reflux

With sulfuric acid; hydrazine hydrate; triethylamine; sodium hydroxide; In ethanol; acetonitrile;
DOI:10.1016/j.bmc.2013.04.022