2,2-dimethyl-exo-3-(2-(2,4,6-trimethoxyphenyl)ethyl)bicyclo<3.2.0>heptan-3-endo-ol

Base Information

Chemical Name:2,2-dimethyl-exo-3-(2-(2,4,6-trimethoxyphenyl)ethyl)bicyclo<3.2.0>heptan-3-endo-ol
CAS No.:106800-21-9
Molecular Formula:C₂₀H₃₀O₄
Molecular Weight:334.456
Hs Code.:

Synonyms:2,2-dimethyl-exo-3-(2-(2,4,6-trimethoxyphenyl)ethyl)bicyclo<3.2.0>heptan-3-endo-ol

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Chemical Property of 2,2-dimethyl-exo-3-(2-(2,4,6-trimethoxyphenyl)ethyl)bicyclo<3.2.0>heptan-3-endo-ol

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Technology Process of 2,2-dimethyl-exo-3-(2-(2,4,6-trimethoxyphenyl)ethyl)bicyclo<3.2.0>heptan-3-endo-ol

There total 6 articles about 2,2-dimethyl-exo-3-(2-(2,4,6-trimethoxyphenyl)ethyl)bicyclo<3.2.0>heptan-3-endo-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 106800-20-8
1-(2,4,6-trimethoxyphenyl)-3-allyl-4,4-dimethylhex-5-en-3-ol

: 106800-21-9
2,2-dimethyl-exo-3-(2-(2,4,6-trimethoxyphenyl)ethyl)bicyclo<3.2.0>heptan-3-endo-ol

Guidance literature:: With copper(I) trifluoromethanesulfonate benzene; In benzene; for 3h; Irradiation;
DOI:10.1021/jo00382a018

Reference yield:

: 830-79-5
2,4,6-trimethoxybenzaldehyde

: 106800-21-9
2,2-dimethyl-exo-3-(2-(2,4,6-trimethoxyphenyl)ethyl)bicyclo<3.2.0>heptan-3-endo-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C to RT

2: 97 percent / Et₃SiH, CF₃COOH / CH₂Cl₂ / 1.5 h / -78 - 20 °C

3: 2.) 10percent HCl, H₂O / 1.) THF, 30 min, 2.) THF, reflux, 30 min

4: 90 percent / diethyl ether / 0.5 h

5: 75 percent / (CuOTf)2*C₆H₆ / benzene / 3 h / Irradiation

With hydrogenchloride; triethylsilane; n-butyllithium; copper(I) trifluoromethanesulfonate benzene; water; trifluoroacetic acid; In diethyl ether; dichloromethane; benzene;
DOI:10.1021/jo00382a018

Reference yield:

: 42924-30-1
3-(2,4,6-trimethoxy-phenyl)-propionitrile

: 106800-21-9
2,2-dimethyl-exo-3-(2-(2,4,6-trimethoxyphenyl)ethyl)bicyclo<3.2.0>heptan-3-endo-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) 10percent HCl, H₂O / 1.) THF, 30 min, 2.) THF, reflux, 30 min

2: 90 percent / diethyl ether / 0.5 h

3: 75 percent / (CuOTf)2*C₆H₆ / benzene / 3 h / Irradiation

With hydrogenchloride; copper(I) trifluoromethanesulfonate benzene; water; In diethyl ether; benzene;
DOI:10.1021/jo00382a018