N-(phenylseleno)ethyl-2α-(2',2'-dimethylvinyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

Base Information

Chemical Name:N-(phenylseleno)ethyl-2α-(2',2'-dimethylvinyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine
CAS No.:235093-69-3
Molecular Formula:C₂₃H₃₅NOSe
Molecular Weight:420.497
Hs Code.:

Synonyms:N-(phenylseleno)ethyl-2α-(2',2'-dimethylvinyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

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Chemical Property of N-(phenylseleno)ethyl-2α-(2',2'-dimethylvinyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

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Technology Process of N-(phenylseleno)ethyl-2α-(2',2'-dimethylvinyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

There total 6 articles about N-(phenylseleno)ethyl-2α-(2',2'-dimethylvinyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 107-86-8
3,3-dimethyl acrylaldehyde

: 235093-65-9
N-(phenylseleno)ethyl-8-aminomenthol

: 235093-69-3
N-(phenylseleno)ethyl-2α-(2',2'-dimethylvinyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

Guidance literature:: In benzene; for 72h; Heating;
DOI:10.1021/jo9816921

Reference yield:

: 115156-56-4
(1R,2S,5R)-5-methyl-2-<1-methyl-1-(benzylamino)ethyl>cyclohexan-1-ol

: 235093-69-3
N-(phenylseleno)ethyl-2α-(2',2'-dimethylvinyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / H₂ / Pd/C / ethanol / 24 h / 7600 Torr

2: 99 percent / CH₂Cl₂ / 18 h / Ambient temperature

3: 92 percent / NaBH₄, BF₃*Et₂O / tetrahydrofuran / 8 h / Ambient temperature

4: 85 percent / benzene / 72 h / Heating

With sodium tetrahydroborate; boron trifluoride diethyl etherate; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; benzene;
DOI:10.1021/jo9816921

Reference yield:

: 1666-13-3
diphenyl diselenide

: 235093-69-3
N-(phenylseleno)ethyl-2α-(2',2'-dimethylvinyl)-4,4,7α-trimethyl-trans-octahydro-1,3-benzoxazine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Br₂ / 1.) THF, 15 min, 2.) 10 min

2: 99 percent / CH₂Cl₂ / 18 h / Ambient temperature

3: 92 percent / NaBH₄, BF₃*Et₂O / tetrahydrofuran / 8 h / Ambient temperature

4: 85 percent / benzene / 72 h / Heating

With sodium tetrahydroborate; boron trifluoride diethyl etherate; bromine; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1021/jo9816921