benzyl 3-(5'-benzyloxy-2'-methoxycarbonyl-3'-propylphenoxy)-6-hydroxy-4-methoxy-2-pentylbenzoate

Base Information

Chemical Name:benzyl 3-(5'-benzyloxy-2'-methoxycarbonyl-3'-propylphenoxy)-6-hydroxy-4-methoxy-2-pentylbenzoate
CAS No.:203206-47-7
Molecular Formula:C₃₈H₄₂O₈
Molecular Weight:626.747
Hs Code.:

Synonyms:benzyl 3-(5'-benzyloxy-2'-methoxycarbonyl-3'-propylphenoxy)-6-hydroxy-4-methoxy-2-pentylbenzoate

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Chemical Property of benzyl 3-(5'-benzyloxy-2'-methoxycarbonyl-3'-propylphenoxy)-6-hydroxy-4-methoxy-2-pentylbenzoate

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Technology Process of benzyl 3-(5'-benzyloxy-2'-methoxycarbonyl-3'-propylphenoxy)-6-hydroxy-4-methoxy-2-pentylbenzoate

There total 3 articles about benzyl 3-(5'-benzyloxy-2'-methoxycarbonyl-3'-propylphenoxy)-6-hydroxy-4-methoxy-2-pentylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 203206-46-6
4-benzyloxy-2-(3'-benzyloxycarbonyl-4'-hydroxy-6'-methoxy-2'-pentylphenoxy)-6-propylbenzoic acid

: 203206-47-7
benzyl 3-(5'-benzyloxy-2'-methoxycarbonyl-3'-propylphenoxy)-6-hydroxy-4-methoxy-2-pentylbenzoate

Guidance literature:: In diethyl ether; ethyl acetate; for 0.0666667h; Ambient temperature;
DOI:10.1071/C97083

Reference yield:

: 124281-31-8
benzyl 3,6-dihydroxy-4-methoxy-2-pentylbenzoate

: 203206-47-7
benzyl 3-(5'-benzyloxy-2'-methoxycarbonyl-3'-propylphenoxy)-6-hydroxy-4-methoxy-2-pentylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / dicyclohexylcarbodiimide / toluene / 24 h / Ambient temperature

2: 13 percent / potassium carbonate / dimethylsulfoxide / 48 h / 75 °C

3: 95 percent / ethyl acetate; diethyl ether / 0.07 h / Ambient temperature

With potassium carbonate; dicyclohexyl-carbodiimide; In diethyl ether; dimethyl sulfoxide; ethyl acetate; toluene;
DOI:10.1071/C97083

Reference yield:

: 203206-45-5
benzyl 3-(4'-benzyloxy-2'-hydroxy-6'-propylbenzoyloxy)-6-hydroxy-4-methoxy-2-pentylbenzoate

: 203206-47-7
benzyl 3-(5'-benzyloxy-2'-methoxycarbonyl-3'-propylphenoxy)-6-hydroxy-4-methoxy-2-pentylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 13 percent / potassium carbonate / dimethylsulfoxide / 48 h / 75 °C

2: 95 percent / ethyl acetate; diethyl ether / 0.07 h / Ambient temperature

With potassium carbonate; In diethyl ether; dimethyl sulfoxide; ethyl acetate;
DOI:10.1071/C97083