benzyl 3,6-dihydroxy-4-methoxy-2-pentylbenzoate

Base Information

Chemical Name:benzyl 3,6-dihydroxy-4-methoxy-2-pentylbenzoate
CAS No.:124281-31-8
Molecular Formula:C₂₀H₂₄O₅
Molecular Weight:344.408
Hs Code.:

Synonyms:

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Chemical Property of benzyl 3,6-dihydroxy-4-methoxy-2-pentylbenzoate

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Technology Process of benzyl 3,6-dihydroxy-4-methoxy-2-pentylbenzoate

There total 7 articles about benzyl 3,6-dihydroxy-4-methoxy-2-pentylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53530-17-9
ethyl 2,4-dimethoxy-6-pentylbenzoate

: 124281-31-8
benzyl 3,6-dihydroxy-4-methoxy-2-pentylbenzoate

Guidance literature:: Multi-step reaction with 8 steps

1: 84 percent / SnCl₄ / CH₂Cl₂ / 2 h / Ambient temperature

2: 92 percent / BCl₃ / CH₂Cl₂ / 0.5 h / -78 °C

3: 53 percent / sodium / 20 h / 120 - 130 °C

4: 82 percent / K₂CO₃ / acetone / 20 h / Heating

5: m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / Ambient temperature

6: 10percent aq. KOH / methanol / 0.75 h / 0 °C

7: H₂ / 10percent Pd/C / ethyl acetate / 16 h

8: diethyl ether / 2 h / Ambient temperature

With potassium hydroxide; hydrogen; sodium; boron trichloride; tin(IV) chloride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; ethyl acetate; acetone;

Reference yield:

: 124281-26-1
ethyl 3-formyl-6-hydroxy-4-methoxy-2-pentylbenzoate

: 124281-31-8
benzyl 3,6-dihydroxy-4-methoxy-2-pentylbenzoate

Guidance literature:: Multi-step reaction with 6 steps

1: 53 percent / sodium / 20 h / 120 - 130 °C

2: 82 percent / K₂CO₃ / acetone / 20 h / Heating

3: m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / Ambient temperature

4: 10percent aq. KOH / methanol / 0.75 h / 0 °C

5: H₂ / 10percent Pd/C / ethyl acetate / 16 h

6: diethyl ether / 2 h / Ambient temperature

With potassium hydroxide; hydrogen; sodium; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; ethyl acetate; acetone;

Reference yield:

: 124281-24-9
ethyl 3-formyl-4,6-dimethoxy-2-pentylbenzoate

: 124281-31-8
benzyl 3,6-dihydroxy-4-methoxy-2-pentylbenzoate

Guidance literature:: Multi-step reaction with 7 steps

1: 92 percent / BCl₃ / CH₂Cl₂ / 0.5 h / -78 °C

2: 53 percent / sodium / 20 h / 120 - 130 °C

3: 82 percent / K₂CO₃ / acetone / 20 h / Heating

4: m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / Ambient temperature

5: 10percent aq. KOH / methanol / 0.75 h / 0 °C

6: H₂ / 10percent Pd/C / ethyl acetate / 16 h

7: diethyl ether / 2 h / Ambient temperature

With potassium hydroxide; hydrogen; sodium; boron trichloride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; ethyl acetate; acetone;