2,3-bis(4-methoxyphenyl)-5-hydroxyquinoxaline

Base Information

Chemical Name:2,3-bis(4-methoxyphenyl)-5-hydroxyquinoxaline
CAS No.:1338054-03-7
Molecular Formula:C₂₂H₁₈N₂O₃
Molecular Weight:358.397
Hs Code.:

Synonyms:2,3-bis(4-methoxyphenyl)-5-hydroxyquinoxaline

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Chemical Property of 2,3-bis(4-methoxyphenyl)-5-hydroxyquinoxaline

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Technology Process of 2,3-bis(4-methoxyphenyl)-5-hydroxyquinoxaline

There total 1 articles about 2,3-bis(4-methoxyphenyl)-5-hydroxyquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 603-85-0
2-Amino-3-nitrophenol

: 1226-42-2
1,2-bis(4-methoxyphenyl)-1,2-ethanedione

: 1338054-03-7
2,3-bis(4-methoxyphenyl)-5-hydroxyquinoxaline

Guidance literature:: 2-Amino-3-nitrophenol; With hydrogenchloride; zinc; In ethanol; water; for 14h; Reflux;

1,2-bis(4-methoxyphenyl)-1,2-ethanedione; In ethanol; for 16h; Reflux;
DOI:10.1039/c1dt10707k

Reference yield: 96.0%

: [iridium(III)(μ-chloro)(2-phenylpyridine)2]2

: 1338054-03-7
2,3-bis(4-methoxyphenyl)-5-hydroxyquinoxaline

: [Ir(2-phenylpyridine)2(2,3-bis(4-methoxyphenyl)-5-hydroxyquinoxaline^(1-))]

Guidance literature:: With Na₂CO₃; In 2-methoxy-ethanol; mixt. of Ir complex, quinoxaline deriv. and Na2CO3 in 2-methoxyethanol heated at 120°C for 16 h; evapn. under vac., residue dissolved in CH2Cl2, washed with water and brine, dried over MgSO4, filtrate concd. under vac., Et2O added, ppt. sepd. and dried under vac.;
DOI:10.1039/c1dt10707k

Reference yield: 88.0%

: 1338054-03-7
2,3-bis(4-methoxyphenyl)-5-hydroxyquinoxaline

: 5970-45-6
zinc(II) acetate dihydrate

: 1374879-41-0
Zn(OC₆H₃N₂C₂(C₆H₄OCH₃)2)2

Guidance literature:: With Na₂CO₃; In 2-methoxy-ethanol; using vac. line and Schlenk techniques; Zn acetate and quinolxaline deriv. with Na2CO3 and 2-methoxyethanol heated at 110°C for 14 h; cooled to room temp.; pptd. by addn. of water; filtered, washed with water, dried in vac.;
DOI:10.1016/j.ica.2012.01.008