Benzoic acid, 4-cyano-2-(methylamino)-, methyl ester (9CI)

Base Information

• Chemical Name: Benzoic acid, 4-cyano-2-(methylamino)-, methyl ester (9CI)
• CAS No.: 64630-03-1
• Molecular Formula: C10H10 N2 O2
• Molecular Weight: 190.1986
• Mol file: 64630-03-1.mol

Synonyms:Benzoic acid, 4-cyano-2-(methylamino)-, methyl ester (9CI)

Chemical Property of Benzoic acid, 4-cyano-2-(methylamino)-, methyl ester (9CI)

Chemical Property:

• Melting Point: 121.5 °C (hexane)
• PSA: 62.12000
• LogP: 1.45958

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 4-cyano-2-(methylamino)-, methyl ester (9CI)

There total 1 articles about Benzoic acid, 4-cyano-2-(methylamino)-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methyl-4-cyano-N-benzyloxycarbonyl-N-methylanthranilat → Methyl-4-cyano-N-methylanthranilat (64630-03-1)

Guidance literature:

With hydrogen bromide; In acetic acid;

DOI:10.1021/ja00462a041

Reference yield:

Methyl-4-cyano-N-methylanthranilat (64630-03-1) → 4-Cyano-N-methylanthranilsaeurehydrazid (64630-04-2)

Guidance literature:

With hydrazine; In methanol; chloroform;

DOI:10.1021/ja00462a041

Reference yield:

Methyl-4-cyano-N-methylanthranilat (64630-03-1) + 2,4-Dichloro-5-nitropyrimidine (49845-33-2) → C14H10ClN5O4

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; at 50 ℃;

DOI:10.1016/j.bmcl.2020.126948

Downstream raw materials:

4-Cyano-N-methylanthranilsaeurehydrazid

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