2-oxo-cyclohexanecarboxylic acid p-toluidide

Base Information

Chemical Name:2-oxo-cyclohexanecarboxylic acid p-toluidide
CAS No.:126486-35-9
Molecular Formula:C₁₄H₁₇NO₂
Molecular Weight:231.294
Hs Code.:

2-oxo-cyclohexanecarboxylic acid <i>p</i>-toluidide

Synonyms:2-oxo-cyclohexanecarboxylic acid p-toluidide

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Chemical Property of 2-oxo-cyclohexanecarboxylic acid p-toluidide

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Technology Process of 2-oxo-cyclohexanecarboxylic acid p-toluidide

There total 1 articles about 2-oxo-cyclohexanecarboxylic acid p-toluidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 106-49-0,12221-03-3
p-toluidine

: 1655-07-8
ethyl 2-oxocyclohexane carboxylate

: 126486-35-9
2-oxo-cyclohexanecarboxylic acid p-toluidide

Guidance literature:: With dmap; In toluene; for 20h; Heating;
DOI:10.1055/s-1989-27383

Reference yield: 94.0%

: 126486-35-9
2-oxo-cyclohexanecarboxylic acid p-toluidide

: 94-36-0
dibenzoyl peroxide

: C₂₁H₂₁NO₄

Guidance literature:: With 2,6-di-tert-butyl-4-methyl-phenol; CHF₃O₃S*C₁₀H₂₄N₂; In chloroform; at 20 ℃; enantioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/ol503592n

Reference yield: 80.0%

: 126486-35-9
2-oxo-cyclohexanecarboxylic acid p-toluidide

: C₁₄H₁₇NO₃

Guidance literature:: With 2,2,2-Trifluoroacetophenone; dihydrogen peroxide; C₈H₂₀N₂*C₂HF₆NO₄S₂; In water; 1,2-dichloro-ethane; toluene; at 20 ℃; for 4h; enantioselective reaction;
DOI:10.1021/jacs.0c11787