cyclopentyl N-[2-(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}phenyl)ethyl]-2-methylalaninate

Base Information

Chemical Name:cyclopentyl N-[2-(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}phenyl)ethyl]-2-methylalaninate
CAS No.:1351815-75-2
Molecular Formula:C₄₃H₅₀N₂O₅
Molecular Weight:674.88
Hs Code.:

Synonyms:cyclopentyl N-[2-(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}phenyl)ethyl]-2-methylalaninate

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Chemical Property of cyclopentyl N-[2-(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}phenyl)ethyl]-2-methylalaninate

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Technology Process of cyclopentyl N-[2-(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}phenyl)ethyl]-2-methylalaninate

There total 9 articles about cyclopentyl N-[2-(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}phenyl)ethyl]-2-methylalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 912545-08-5
2,4-bis-benzyloxy-5-isopropenyl-benzoic acid methyl ester

: 1351815-75-2
cyclopentyl N-[2-(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}phenyl)ethyl]-2-methylalaninate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide; methanol / 20 h / 75 °C

1.2: 0.5 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 18 h / 20 °C

3.1: Dess-Martin periodane / dichloromethane / 0.5 h

4.1: sodium tris(acetoxy)borohydride / 1,1-dichloroethane / 1 h

With methanol; sodium tris(acetoxy)borohydride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; HATU; potassium hydroxide; In 1,1-dichloroethane; dichloromethane;

Reference yield:

: cyclopentyl 2-methylalaninate

: C₃₄H₃₃NO₄

: 1351815-75-2
cyclopentyl N-[2-(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}phenyl)ethyl]-2-methylalaninate

Guidance literature:: cyclopentyl 2-methylalaninate; C₃₄H₃₃NO₄; With sodium tris(acetoxy)borohydride; In 1,1-dichloroethane; for 1h;

With ammonium chloride; In 1,1-dichloroethane;

Reference yield:

: 2150-47-2
methyl 2,4-dihydroxybenzoate

: 1351815-75-2
cyclopentyl N-[2-(4-{[{[2,4-bis(benzyloxy)-5-(prop-1-en-2-yl)phenyl]carbonyl}(methyl)amino]methyl}phenyl)ethyl]-2-methylalaninate

Guidance literature:: Multi-step reaction with 8 steps

1.1: dmap / 1 h / 55 °C

2.1: trifluorormethanesulfonic acid / toluene / 2.5 h / 20 °C / Cooling with ice

2.2: 18 h / 20 °C

3.1: potassium carbonate / acetonitrile / 42 h / 75 °C

4.1: potassium tert-butylate / tetrahydrofuran / 0.5 h

4.2: 0.5 h

5.1: potassium hydroxide; methanol / 20 h / 75 °C

5.2: 0.5 h / 20 °C

6.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 18 h / 20 °C

7.1: Dess-Martin periodane / dichloromethane / 0.5 h

8.1: sodium tris(acetoxy)borohydride / 1,1-dichloroethane / 1 h

With methanol; trifluorormethanesulfonic acid; potassium tert-butylate; sodium tris(acetoxy)borohydride; potassium carbonate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; HATU; potassium hydroxide; dmap; In tetrahydrofuran; 1,1-dichloroethane; dichloromethane; toluene; acetonitrile;