O-4-Amino-(4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-α-D-glucopyranosyl-(1->4)-α-D-glucopyranose

Base Information

• Chemical Name: O-4-Amino-(4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-α-D-glucopyranosyl-(1->4)-α-D-glucopyranose
• CAS No.: 92567-71-0
• Molecular Formula: C₁₈H₃₃NO₁₄
• Molecular Weight: 487.458

Synonyms:O-4-Amino-(4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-α-D-glucopyranosyl-(1->4)-α-D-glucopyranose

Chemical Property of O-4-Amino-(4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-α-D-glucopyranosyl-(1->4)-α-D-glucopyranose

Chemical Property:

Purity/Quality:

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Technology Process of O-4-Amino-(4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-α-D-glucopyranosyl-(1->4)-α-D-glucopyranose

There total 5 articles about O-4-Amino-(4,6-didesoxy-α-D-glucopyranosyl)-(1->4)-O-α-D-glucopyranosyl-(1->4)-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acarbose (56180-94-0,68107-33-5,106864-09-9) → (3R,4R,5S,6R)-5-[(2R,3R,4R,5S,6R)-5-((2R,3R,4S,5S,6R)-5-Amino-3,4-dihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-3,4-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-6-hydroxymethyl-tetrahydro-pyran-2,3,4-triol (92567-53-8,92567-71-0) + C25H45NO18 (85382-75-8,85440-60-4,92621-52-8,92621-65-3)

Guidance literature:

With hydrogen; triethylamine; nickel; In water; at 25 ℃; for 20h; under 750.06 Torr; Yield given. Yields of byproduct given; pH 8;

DOI:10.1016/0008-6215(91)80045-O

Reference yield:

acarbose (56180-94-0,68107-33-5,106864-09-9) → (3R,4R,5S,6R)-5-[(2R,3R,4R,5S,6R)-5-((2R,3R,4S,5S,6R)-5-Amino-3,4-dihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-3,4-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-6-hydroxymethyl-tetrahydro-pyran-2,3,4-triol (92567-53-8,92567-71-0) + 1D-(1,3/2,4)-1-Hydroxymethyl-2,3,4-cyclohexantriol (76703-50-9) + dihydroacarbose (85382-75-8,85440-60-4,92621-52-8,92621-65-3) + C25H45NO18 (85382-75-8,85440-60-4,92621-52-8,92621-65-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In water; at 25 ℃; for 20h; under 750.06 Torr; Yield given. Further byproducts given. Yields of byproduct given;

DOI:10.1016/0008-6215(91)80045-O

Reference yield:

acarbose (56180-94-0,68107-33-5,106864-09-9) → 5a-carba-1,5-anhydro-L-iditol (139561-46-9) + (3R,4R,5S,6R)-5-[(2R,3R,4R,5S,6R)-5-((2R,3R,4S,5S,6R)-5-Amino-3,4-dihydroxy-6-methyl-tetrahydro-pyran-2-yloxy)-3,4-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy]-6-hydroxymethyl-tetrahydro-pyran-2,3,4-triol (92567-53-8,92567-71-0) + dihydroacarbose (85382-75-8,85440-60-4,92621-52-8,92621-65-3) + C25H45NO18 (85382-75-8,85440-60-4,92621-52-8,92621-65-3)

Guidance literature:

With hydrogen; nickel; In water; at 25 ℃; for 20h; under 750.06 Torr; Yield given. Further byproducts given. Yields of byproduct given; pH 3;

DOI:10.1016/0008-6215(91)80045-O

upstream raw materials:

acarbose

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