C₃₆H₅₀BrN₅O₆SSi₂

Base Information

Chemical Name:C₃₆H₅₀BrN₅O₆SSi₂
CAS No.:1402170-36-8
Molecular Formula:C₃₆H₅₀BrN₅O₆SSi₂
Molecular Weight:816.964
Hs Code.:

C<sub>36</sub>H<sub>50</sub>BrN<sub>5</sub>O<sub>6</sub>SSi<sub>2</sub>

Synonyms:C₃₆H₅₀BrN₅O₆SSi₂

Suppliers and Price of C₃₆H₅₀BrN₅O₆SSi₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₆H₅₀BrN₅O₆SSi₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₆H₅₀BrN₅O₆SSi₂

There total 12 articles about C₃₆H₅₀BrN₅O₆SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.7%

: 1402170-35-7
C₃₆H₅₂BrN₅O₇SSi₂

: 1402170-36-8
C₃₆H₅₀BrN₅O₆SSi₂

Guidance literature:: With tributylphosphine; diamide; In toluene; at 20 ℃; for 1.16667h; Inert atmosphere; Reflux;
DOI:10.1002/anie.201204726

Reference yield:

: 1402170-30-2
C₂₈H₅₆N₂O₃Si₃

: 1402170-36-8
C₃₆H₅₀BrN₅O₆SSi₂

Guidance literature:: Multi-step reaction with 8 steps

1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenylphosphine; copper(l) iodide; N-butylamine / toluene / 1.17 h / Inert atmosphere; Reflux

2: sodium methylate / tetrahydrofuran; methanol / 0.5 h / 20 - 50 °C / Inert atmosphere

3: zinc; hydrogenchloride / water; methanol / 0.67 h / 20 °C / Reflux

4: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

5: zinc; ammonium chloride / ethanol / 0.33 h / 20 °C

6: pyridine / dichloromethane / 2 h / 0 °C / Inert atmosphere

7: camphor-10-sulfonic acid / methanol / 0.67 h / 20 - 50 °C

8: diamide; tributylphosphine / toluene / 1.17 h / 20 °C / Inert atmosphere; Reflux

With pyridine; hydrogenchloride; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; copper(l) iodide; tributylphosphine; diamide; camphor-10-sulfonic acid; sodium methylate; sodium hydride; ammonium chloride; N-butylamine; triphenylphosphine; zinc; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 1: |Sonogashira Cross-Coupling;
DOI:10.1002/anie.201204726

Reference yield:

: 1402170-32-4
C₃₆H₆₂BrN₃O₃Si₃

: 1402170-36-8
C₃₆H₅₀BrN₅O₆SSi₂

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.33 h / 0 °C / Inert atmosphere

2: zinc; ammonium chloride / ethanol / 0.33 h / 20 °C

3: pyridine / dichloromethane / 2 h / 0 °C / Inert atmosphere

4: camphor-10-sulfonic acid / methanol / 0.67 h / 20 - 50 °C

5: diamide; tributylphosphine / toluene / 1.17 h / 20 °C / Inert atmosphere; Reflux

With pyridine; tributylphosphine; diamide; camphor-10-sulfonic acid; sodium hydride; ammonium chloride; zinc; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/anie.201204726