N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylserine

Base Information

Chemical Name:N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylserine
CAS No.:102249-08-1
Molecular Formula:C₂₈H₃₄N₈O₉
Molecular Weight:626.626
Hs Code.:

N<sup>α</sup>-benzyloxycarbonyltryptophyl-N<sup>G</sup>-nitroarginylserine

Synonyms:N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylserine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylserine

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Technology Process of N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylserine

There total 4 articles about N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylserine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 102249-07-0
N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylserine methyl ester

: 102249-08-1
N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylserine

Guidance literature:: With sodium hydroxide; In ethanol; at 18 ℃; for 1h;

Reference yield:

: 2304-98-5
N₅-[imino(nitroamino)methyl]-N₂-[(phenylmethoxy)carbonyl]-L-ornithine

: 102249-08-1
N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylserine

Guidance literature:: Multi-step reaction with 4 steps

1: 1) Et₃N, isobutyl chloroformate or pivaloyl chloride 2) Et₃N / 1) CHCl₃, -10 deg C 2) 0 deg C, 1 h, then 18-25 deg C, 16 h

2: 40percent HBr / acetic acid / 2 h / 20 °C

3: 20 percent / Et₃N / dimethylformamide / 24 h / 18 - 25 °C

4: 36 percent / 2N-NaOH / ethanol / 1 h / 18 °C

With sodium hydroxide; hydrogen bromide; pivaloyl chloride; triethylamine; isobutyl chloroformate; In ethanol; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: C₁₀H₂₀N₆O₆

: 102249-08-1
N^α-benzyloxycarbonyltryptophyl-N^G-nitroarginylserine

Guidance literature:: Multi-step reaction with 2 steps

1: 20 percent / Et₃N / dimethylformamide / 24 h / 18 - 25 °C

2: 36 percent / 2N-NaOH / ethanol / 1 h / 18 °C

With sodium hydroxide; triethylamine; In ethanol; N,N-dimethyl-formamide;