(+)-(1'R,2'R,3'S)-4-(2',3'-Epoxy-2',6',6'-trimethylcyclohex-1'-yl)but-3-en-2-on

Base Information

• Chemical Name: (+)-(1'R,2'R,3'S)-4-(2',3'-Epoxy-2',6',6'-trimethylcyclohex-1'-yl)but-3-en-2-on
• CAS No.: 108944-32-7
• Molecular Formula: C₁₃H₂₀O₂
• Molecular Weight: 208.301

Synonyms:(+)-(1'R,2'R,3'S)-4-(2',3'-Epoxy-2',6',6'-trimethylcyclohex-1'-yl)but-3-en-2-on

Chemical Property of (+)-(1'R,2'R,3'S)-4-(2',3'-Epoxy-2',6',6'-trimethylcyclohex-1'-yl)but-3-en-2-on

Chemical Property:

Purity/Quality:

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Technology Process of (+)-(1'R,2'R,3'S)-4-(2',3'-Epoxy-2',6',6'-trimethylcyclohex-1'-yl)but-3-en-2-on

There total 14 articles about (+)-(1'R,2'R,3'S)-4-(2',3'-Epoxy-2',6',6'-trimethylcyclohex-1'-yl)but-3-en-2-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

alpha-ionone (127-41-3,6901-97-9,14398-36-8,24190-29-2,30685-95-1,31798-12-6,52340-45-1,67529-94-6,67529-95-7) → (rac)-4-(2,3-epoxy-2,6,6-trimethylcyclohexyl)-3-buten-2-one (37677-81-9,72523-51-4,72523-52-5,73925-68-5,84107-27-7,84107-28-8,97371-49-8,108944-32-7,108944-33-8,809237-15-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 0 ℃; for 12h;

DOI:10.1039/c39850000421

Reference yield: 87.0%

alpha-ionone (127-41-3,6901-97-9,14398-36-8,24190-29-2,30685-95-1,31798-12-6,52340-45-1,67529-94-6,67529-95-7) → 4-(2,3-epoxy-2,6,6-trimethylcyclohexyl)-3-buten-2-one (37677-81-9,72523-51-4,72523-52-5,73925-68-5,84107-27-7,84107-28-8,97371-49-8,108944-32-7,108944-33-8,809237-15-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid;

Reference yield: 57.0%

(+)-(R)-α-Ionon (24190-29-2) → (+)-(1'R,2'S,3'R)-4-(2',3'-Epoxy-2',6',6'-trimethylcyclohex-1'-yl)but-3-en-2-on (108944-33-8,809237-15-8) + (+)-(1'R,2'R,3'S)-4-(2',3'-Epoxy-2',6',6'-trimethylcyclohex-1'-yl)but-3-en-2-on (108944-32-7,809237-15-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 12h; Ambient temperature;

DOI:10.1002/hlca.19860690409

upstream raw materials:

alpha-ionone

(+)-(R)-α-Ionon

(R)-α-ionone

Downstream raw materials:

4-(3-hydroxy-2,6,6-trimethylcyclohex-1-enyl)but-3-en-2-one

7-hydroxy-4,6,10,10-tetramethyl-5-oxatricyclo<4.4.0.0^1.4>dec-2-ene

(Z,1'RS,2'RS,3'SR)-4-(2',3'-epoxy-2',6',6'-trimethylcyclohexyl)-3-buten-2-one

4-Hydroxy-1.1.3-trimethyl-2-(3-hydroxy-butyl)-cyclohexan

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