[VO(OEt)(2-hydroxybenzoylhydrazine 2-hydroxybenzoylhydrazone(-2H))]

Base Information

Chemical Name:[VO(OEt)(2-hydroxybenzoylhydrazine 2-hydroxybenzoylhydrazone(-2H))]
CAS No.:897627-58-6
Molecular Formula:C₂H₅O*C₁₄H₉N₂O₃*H*OV
Molecular Weight:366.247
Hs Code.:

Synonyms:[VO(OEt)(2-hydroxybenzoylhydrazine 2-hydroxybenzoylhydrazone(-2H))]

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Chemical Property of [VO(OEt)(2-hydroxybenzoylhydrazine 2-hydroxybenzoylhydrazone(-2H))]

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Technology Process of [VO(OEt)(2-hydroxybenzoylhydrazine 2-hydroxybenzoylhydrazone(-2H))]

There total 1 articles about [VO(OEt)(2-hydroxybenzoylhydrazine 2-hydroxybenzoylhydrazone(-2H))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 3153-26-2
bis(acetylacetonate)oxovanadium

: 3232-36-8
salicylidene salicylhydrazide

: 897627-58-6
[VO(OEt)(2-hydroxybenzoylhydrazine 2-hydroxybenzoylhydrazone(-2H))]

Guidance literature:: With air; In ethanol; V complex added to a soln. of ligand, stirred for 6 h in open air; filtered, crystd. for 3 d; elem. anal.;
DOI:10.1021/ic051120g

Reference yield: 80.0%

: 897627-58-6
[VO(OEt)(2-hydroxybenzoylhydrazine 2-hydroxybenzoylhydrazone(-2H))]

: 13362-78-2
trans-1,2-bis(pyridin-4-yl)ethene

: [VO(OEt)(2-hydroxybenzoylhydrazine 2-hydroxybenzoylhydrazone(-2H))]2(μ-1,2-bis(4-pyridyl)ethylene)

Guidance literature:: In ethanol; ligand added to a soln. of V complex, refluxed; filtered, crystd. on cooling; elem. anal.;
DOI:10.1021/ic051120g

Reference yield: 80.0%

: 822-36-6
4-methyl-1H-imidazole

: 64-17-5
ethanol

: 897627-58-6
[VO(OEt)(2-hydroxybenzoylhydrazine 2-hydroxybenzoylhydrazone(-2H))]

: [4-methyl imidazole(+1H)][VO(2-hydroxybenzoylhydrazine 2-hydroxybenzoylhydrazone(-2H))]

Guidance literature:: In ethanol; 4-methyl imidazole added to a soln. of V complex, refluxed for 5 h; filtered, crystd. for 4-5 d at room temp., recrystd. (MeOH); elem. anal.;
DOI:10.1021/ic051120g