Technology Process of C24H23NO4
There total 5 articles about C24H23NO4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C20H19NO2;
With
lithium diisopropyl amide;
In
tetrahydrofuran;
at -78 ℃;
for 1h;
Inert atmosphere;
Allyl chloroformate;
In
tetrahydrofuran;
at -78 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/jo402741g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / toluene
2.1: palladium diacetate; copper diacetate; potassium carbonate / N,N-dimethyl-formamide / 3 h / 140 °C
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C
3.2: 2 h / 0 - 20 °C
4.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
4.2: 1 h / -78 °C / Inert atmosphere
With
copper diacetate; palladium diacetate; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; lithium diisopropyl amide;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/jo402741g
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: palladium diacetate; copper diacetate; potassium carbonate / N,N-dimethyl-formamide / 3 h / 140 °C
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 0 - 20 °C
2.2: 2 h / 0 - 20 °C
3.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
3.2: 1 h / -78 °C / Inert atmosphere
With
copper diacetate; palladium diacetate; sodium hydride; potassium carbonate; lithium diisopropyl amide;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo402741g
