1-(1-(4-((allyloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethylpiperidine

Base Information

Chemical Name:1-(1-(4-((allyloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethylpiperidine
CAS No.:1431328-82-3
Molecular Formula:C₂₃H₃₇NO₂
Molecular Weight:359.552
Hs Code.:

Synonyms:1-(1-(4-((allyloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethylpiperidine

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Chemical Property of 1-(1-(4-((allyloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethylpiperidine

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Technology Process of 1-(1-(4-((allyloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethylpiperidine

There total 6 articles about 1-(1-(4-((allyloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1-[1-(4-iodomethyl-phenyl)-2-methyl-propoxy]-2,2,6,6-tetramethyl-piperidine

: 107-18-6
allyl alcohol

: 1431328-82-3
1-(1-(4-((allyloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:: allyl alcohol; With sodium hydride; In tetrahydrofuran; mineral oil; at 70 ℃; for 1h;

1-[1-(4-iodomethyl-phenyl)-2-methyl-propoxy]-2,2,6,6-tetramethyl-piperidine; In tetrahydrofuran; mineral oil; for 24h;
DOI:10.1002/chem.201200499

Reference yield:

: 947769-95-1
4-(1-bromo-2-methylpropyl)-benzaldehyde

: 1431328-82-3
1-(1-(4-((allyloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper; copper(II) bis(trifluoromethanesulfonate); 4,4'-di-tert-butyl-2,2'-bipyridine / benzene / 28 h / 80 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 20 °C

3.1: sodium iodide; chloro-trimethyl-silane / acetonitrile / 6 h / 20 °C

4.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 70 °C

4.2: 24 h

With lithium aluminium tetrahydride; chloro-trimethyl-silane; copper(II) bis(trifluoromethanesulfonate); copper; sodium hydride; 4,4'-di-tert-butyl-2,2'-bipyridine; sodium iodide; In tetrahydrofuran; acetonitrile; mineral oil; benzene;
DOI:10.1002/chem.201200499

Reference yield:

: {4-[2-methyl-1-(2,2,6,6-tetramethyl-piperidin-1-yloxy)-propyl]-phenyl}-methanol

: 1431328-82-3
1-(1-(4-((allyloxy)methyl)phenyl)-2-methylpropoxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium iodide; chloro-trimethyl-silane / acetonitrile / 6 h / 20 °C

2.1: sodium hydride / mineral oil; tetrahydrofuran / 1 h / 70 °C

2.2: 24 h

With chloro-trimethyl-silane; sodium hydride; sodium iodide; In tetrahydrofuran; acetonitrile; mineral oil;
DOI:10.1002/chem.201200499