di-tert-butyl 1[1-benzyl-2-(benzyloxy)ethyl]hydrazine-1,2-dicarboxylate

Base Information

• Chemical Name: di-tert-butyl 1[1-benzyl-2-(benzyloxy)ethyl]hydrazine-1,2-dicarboxylate
• CAS No.: 1132070-41-7
• Molecular Formula: C₂₆H₃₆N₂O₅
• Molecular Weight: 456.582
• Mol file: 1132070-41-7.mol

Synonyms:di-tert-butyl 1[1-benzyl-2-(benzyloxy)ethyl]hydrazine-1,2-dicarboxylate

Chemical Property of di-tert-butyl 1[1-benzyl-2-(benzyloxy)ethyl]hydrazine-1,2-dicarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of di-tert-butyl 1[1-benzyl-2-(benzyloxy)ethyl]hydrazine-1,2-dicarboxylate

There total 1 articles about di-tert-butyl 1[1-benzyl-2-(benzyloxy)ethyl]hydrazine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

di-tert-butyl 1[(1-benzyl-2-hydroxy)ethyl]hydrazine-1,2-dicarboxylate (864922-13-4) + benzyl chloride (100-44-7) → di-tert-butyl 1[1-benzyl-2-(benzyloxy)ethyl]hydrazine-1,2-dicarboxylate (1132070-41-7)

Guidance literature:

With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 80 ℃;

DOI:10.1007/s10593-008-0003-y

Reference yield: 70.0%

malonaldehydebis(dimethylacetal) (102-52-3) + di-tert-butyl 1[1-benzyl-2-(benzyloxy)ethyl]hydrazine-1,2-dicarboxylate (1132070-41-7) → 1-[(1-benzyl-2-benzyloxy)ethyl]-1H-pyrazole

Guidance literature:

In hydrogenchloride; at 70 - 80 ℃;

DOI:10.1007/s10593-008-0003-y

upstream raw materials:

di-tert-butyl 1[(1-benzyl-2-hydroxy)ethyl]hydrazine-1,2-dicarboxylate

benzyl chloride