N⁴-benzoyl-1-(5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-seleno-β-D-ribofuranosyl)cytosine

Base Information

• Chemical Name: N⁴-benzoyl-1-(5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-seleno-β-D-ribofuranosyl)cytosine
• CAS No.: 1006032-34-3
• Molecular Formula: C₃₅H₃₉N₃O₅SeSi
• Molecular Weight: 688.757

Synonyms:N⁴-benzoyl-1-(5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-seleno-β-D-ribofuranosyl)cytosine

Chemical Property of N⁴-benzoyl-1-(5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-seleno-β-D-ribofuranosyl)cytosine

Chemical Property:

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Technology Process of N⁴-benzoyl-1-(5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-seleno-β-D-ribofuranosyl)cytosine

There total 1 articles about N⁴-benzoyl-1-(5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-seleno-β-D-ribofuranosyl)cytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

C24H32O4SeSi (1006032-31-0) + 4-N-benzoylcytosine (26661-13-2) → N4-benzoyl-1-(5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-seleno-β-D-ribofuranosyl)cytosine (1006032-34-3)

Guidance literature:

4-N-benzoylcytosine; With trimethylsilyl trifluoromethanesulfonate; triethylamine; In toluene; at 20 ℃; for 1h;

C₂₄H₃₂O₄SeSi; With triethylamine; In dichloromethane; toluene; at 0 - 20 ℃; Further stages.;

DOI:10.1021/ol7025558

Reference yield: 100.0%

N4-benzoyl-1-(5-O-tert-butyldiphenylsilyl-2,3-O-isopropylidene-4-seleno-β-D-ribofuranosyl)cytosine (1006032-34-3) → 1-(4-seleno-β-D-ribofuranosyl)-N4-benzoylcytosine (1030021-71-6)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 1h;

DOI:10.1021/jo8003277

upstream raw materials:

C₂₄H₃₂O₄SeSi

4-N-benzoylcytosine

Downstream raw materials:

1-(4-seleno-β-D-ribofuranosyl)-N⁴-benzoylcytosine

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