(S)-2-tert-butoxycarbonylamino-3-[4-(di-tert-butylfluorosilanyl)phenyl]propionic acid

Base Information

Chemical Name:(S)-2-tert-butoxycarbonylamino-3-[4-(di-tert-butylfluorosilanyl)phenyl]propionic acid
CAS No.:1309935-57-6
Molecular Formula:C₂₂H₃₆FNO₄Si
Molecular Weight:425.616
Hs Code.:

Synonyms:(S)-2-tert-butoxycarbonylamino-3-[4-(di-tert-butylfluorosilanyl)phenyl]propionic acid

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Chemical Property of (S)-2-tert-butoxycarbonylamino-3-[4-(di-tert-butylfluorosilanyl)phenyl]propionic acid

Chemical Property:

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Technology Process of (S)-2-tert-butoxycarbonylamino-3-[4-(di-tert-butylfluorosilanyl)phenyl]propionic acid

There total 11 articles about (S)-2-tert-butoxycarbonylamino-3-[4-(di-tert-butylfluorosilanyl)phenyl]propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1309935-54-3
(S)-2-amino-3-[4-(di-tert-butylfluorosilanyl)phenyl]propionic acid

: 1309935-57-6
(S)-2-tert-butoxycarbonylamino-3-[4-(di-tert-butylfluorosilanyl)phenyl]propionic acid

Guidance literature:: With triethylamine; In dichloromethane; acetonitrile; at 20 ℃; for 24h;
DOI:10.1002/ejic.201100142

Reference yield:

: 1309935-52-1
[4-(di-tert-butylfluorosilanyl)phenyl]acetaldehyde

: 1309935-57-6
(S)-2-tert-butoxycarbonylamino-3-[4-(di-tert-butylfluorosilanyl)phenyl]propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonia; ammonium chloride / water / 0 °C

1.2: 0 - 20 °C

1.3: 12 h / Reflux

2.1: α-chymotrypsin / acetonitrile / 24 h / 30 °C / pH 7.8 / aq. phosphate buffer; Enzymatic reaction

3.1: triethylamine / dichloromethane; acetonitrile / 24 h / 20 °C

With ammonia; ammonium chloride; triethylamine; α-chymotrypsin; In dichloromethane; water; acetonitrile;
DOI:10.1002/ejic.201100142

Reference yield:

: 1309935-53-2
methyl rac-2-amino-3-[4-(di-tert-butyl-fluoro-silanyl)-phenyl]-propionate

: 1309935-57-6
(S)-2-tert-butoxycarbonylamino-3-[4-(di-tert-butylfluorosilanyl)phenyl]propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: α-chymotrypsin / acetonitrile / 24 h / 30 °C / pH 7.8 / aq. phosphate buffer; Enzymatic reaction

2: triethylamine / dichloromethane; acetonitrile / 24 h / 20 °C

With triethylamine; α-chymotrypsin; In dichloromethane; acetonitrile;
DOI:10.1002/ejic.201100142