N-[(1S)-1-isobutylbuta-2,3-dienyl]-2,4,6-trimethyl-N-[(E)-3-phenyl-2-propenyl]phenylsulfonamide

Base Information

• Chemical Name: N-[(1S)-1-isobutylbuta-2,3-dienyl]-2,4,6-trimethyl-N-[(E)-3-phenyl-2-propenyl]phenylsulfonamide
• CAS No.: 597540-86-8
• Molecular Formula: C₂₆H₃₃NO₂S
• Molecular Weight: 423.62

Synonyms:N-[(1S)-1-isobutylbuta-2,3-dienyl]-2,4,6-trimethyl-N-[(E)-3-phenyl-2-propenyl]phenylsulfonamide

Chemical Property of N-[(1S)-1-isobutylbuta-2,3-dienyl]-2,4,6-trimethyl-N-[(E)-3-phenyl-2-propenyl]phenylsulfonamide

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Technology Process of N-[(1S)-1-isobutylbuta-2,3-dienyl]-2,4,6-trimethyl-N-[(E)-3-phenyl-2-propenyl]phenylsulfonamide

There total 1 articles about N-[(1S)-1-isobutylbuta-2,3-dienyl]-2,4,6-trimethyl-N-[(E)-3-phenyl-2-propenyl]phenylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

Cinnamyl bromide (4392-24-9) + (4S)-6-methyl-4-[N-(2,4,6-trimethylphenylsulfonyl)amino]hepta-1,2-diene (736948-26-8) → N-[(1S)-1-isobutylbuta-2,3-dienyl]-2,4,6-trimethyl-N-[(E)-3-phenyl-2-propenyl]phenylsulfonamide (597540-86-8)

Guidance literature:

(4S)-6-methyl-4-[N-(2,4,6-trimethylphenylsulfonyl)amino]hepta-1,2-diene; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.166667h;

Cinnamyl bromide; In N,N-dimethyl-formamide; at 0 ℃; for 2h;

DOI:10.1002/chem.200500050

Reference yield: 36.0%

N-[(1S)-1-isobutylbuta-2,3-dienyl]-2,4,6-trimethyl-N-[(E)-3-phenyl-2-propenyl]phenylsulfonamide (597540-86-8) + para-iodoanisole (696-62-8) → (3S,4S,7R,8S)-5-aza-4-isobutyl-11-methoxy-2-methylene-8-phenyl-5-(2,4,6-trimethylphenylsulfonyl)tricyclo[7.4.0.03,7]trideca-1(9),10,12-triene + (3S,4S,7S,8S)-5-aza-4-isobutyl-11-methoxy-2-methylene-8-phenyl-5-(2,4,6-trimethylphenylsulfonyl)tricyclo[7.4.0.03,7]trideca-1(9),10,12-triene

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; for 13h; Heating;

DOI:10.1002/chem.200500050

Reference yield: 21.0%

N-[(1S)-1-isobutylbuta-2,3-dienyl]-2,4,6-trimethyl-N-[(E)-3-phenyl-2-propenyl]phenylsulfonamide (597540-86-8) + iodobenzene (591-50-4) → (3S,4S,7R,8S)-5-aza-4-isobutyl-2-methylene-8-phenyl-5-(2,4,6-trimethylphenylsulfonyl)tricyclo[7.4.0.03,7]trideca-1(9),10,12-triene + (3S,4S,7S,8S)-5-aza-4-isobutyl-2-methylene-8-phenyl-5-(2,4,6-trimethylphenylsulfonyl)tricyclo[7.4.0.03,7]trideca-1(9),10,12-triene

Guidance literature:

With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; for 29h; Heating;

DOI:10.1002/chem.200500050

upstream raw materials:

Cinnamyl bromide

(4S)-6-methyl-4-[N-(2,4,6-trimethylphenylsulfonyl)amino]hepta-1,2-diene

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