(E)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylacrylamide

Base Information

Chemical Name:(E)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylacrylamide
CAS No.:1539220-73-9
Molecular Formula:C₄₁H₄₁NO₃
Molecular Weight:595.781
Hs Code.:

Synonyms:(E)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylacrylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylacrylamide

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Technology Process of (E)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylacrylamide

There total 2 articles about (E)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 23795-34-8
3-phenylpropenoic acid N,N-diisopropylamide

: 1539220-65-9
2-bromo-4-trityloxymethylphenol

: 1539220-73-9
(E)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylacrylamide

Guidance literature:: With bis(tri-t-butylphosphine)palladium⁽⁰⁾; N-Methyldicyclohexylamine; In 2-methyltetrahydrofuran; at 70 - 86 ℃; for 5h; Reflux;

Reference yield:

: 29922-56-3
2-bromo-4-(hydroxymethyl)phenol

: 76-83-5
trityl chloride

: 1539220-73-9
(E)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylacrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine hydrochloride / N,N-dimethyl-formamide

2: N-Methyldicyclohexylamine; bis(tri-t-butylphosphine)palladium⁽⁰⁾ / 2-methyltetrahydrofuran / 5 h / 70 - 86 °C / Reflux

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; N-Methyldicyclohexylamine; pyridine hydrochloride; In 2-methyltetrahydrofuran; N,N-dimethyl-formamide;