bis(2-(diphenylphosphaneyl)-4-methylphenyl)amine

Base Information

Chemical Name:bis(2-(diphenylphosphaneyl)-4-methylphenyl)amine
CAS No.:1011473-19-0
Molecular Formula:C₃₈H₃₃NP₂
Molecular Weight:565.634
Hs Code.:

Synonyms:bis(2-(diphenylphosphaneyl)-4-methylphenyl)amine

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Chemical Property of bis(2-(diphenylphosphaneyl)-4-methylphenyl)amine

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Technology Process of bis(2-(diphenylphosphaneyl)-4-methylphenyl)amine

There total 1 articles about bis(2-(diphenylphosphaneyl)-4-methylphenyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 27996-13-0
α,α'-dibromo-di-p-tolylamine

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 1011473-19-0
bis(2-(diphenylphosphaneyl)-4-methylphenyl)amine

Guidance literature:: α,α'-dibromo-di-p-tolylamine; With n-butyllithium; In diethyl ether; hexane; at -35 - 20 ℃;

chloro-diphenylphosphine; In diethyl ether; hexane; at 20 ℃; for 20h; Further stages.;
DOI:10.1021/ja7105306

Reference yield: 85.0%

: dichloro(1,5-cyclooctadiene)ruthenium(II)

: 1011473-19-0
bis(2-(diphenylphosphaneyl)-4-methylphenyl)amine

: 1263063-31-5
[ruthenium(dichloride)(NH(2-PPh₂-4-Me-C₆H₃)2)]

Guidance literature:: In toluene; Schlenk or glove box techniques, under N2; mixt. of PNP(Ph)H and Ru complex (equimolar amounts) in toluene heated at 110°C for 24 h; ppt. filtered off, dried under vac., elem. anal.;
DOI:10.1016/j.ica.2010.07.040

Reference yield: 84.0%

: chlorobis(cyclooctene)-iridium(I) dimer

: 1011473-19-0
bis(2-(diphenylphosphaneyl)-4-methylphenyl)amine

: 1255934-46-3
(N(2-PPh₂-4-Me-C₆H₃)2)Ir(COE)

Guidance literature:: With LiN(Si(CH₃)3)2; In fluorobenzene; byproducts: LiCl; (N2); a flask loaded with ligand, Li compd. and C6H5F, stirred for 1 h at ambient temp., added to a suspn. of Ir complex, stirred for 1 h; filtered, washed (CH2Cl2), concd., washed (hexanes), filtered, dried (vac.); elem. anal.;
DOI:10.1039/b925856f