Benzenamine, 2-bromo-N-(2-bromo-4-methylphenyl)-4-methyl-

Base Information

• Chemical Name: Benzenamine, 2-bromo-N-(2-bromo-4-methylphenyl)-4-methyl-
• CAS No.: 27996-13-0
• Molecular Formula: C14H13Br2N
• Molecular Weight: 355.072
• Mol file: 27996-13-0.mol

Synonyms:Benzenamine,2-bromo-N-(2-bromo-4-methylphenyl)-4-methyl;bis(2-bromo-4-methylphenyl)amine;(2-Br-p-tolyl)2NH;bis(2-bromo-p-tolyl)amine;HN(2-Br-p-tolyl);di(2-bromo-p-tolyl)amine;Bis-(2-brom-4-methyl-phenyl)-amin;

Chemical Property of Benzenamine, 2-bromo-N-(2-bromo-4-methylphenyl)-4-methyl-

Chemical Property:

• PSA: 12.03000
• LogP: 5.64500

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenamine, 2-bromo-N-(2-bromo-4-methylphenyl)-4-methyl-

There total 2 articles about Benzenamine, 2-bromo-N-(2-bromo-4-methylphenyl)-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

di-p-tolylamine (620-93-9) → α,α'-dibromo-di-p-tolylamine (27996-13-0)

Guidance literature:

With bromine; In methanol; dichloromethane; at 0 ℃;

DOI:10.1016/j.jorganchem.2011.08.013

Reference yield:

→ α,α'-dibromo-di-p-tolylamine (27996-13-0)

Guidance literature:

Di-p-tolyl-amin, Br2, Eg.;

DOI:10.1021/jo01067a110

Reference yield: 97.0%

α,α'-dibromo-di-p-tolylamine (27996-13-0) + benzyl bromide (100-39-0) → N,N-bis(2-bromo-4-methylphenyl)benzylamine (1421946-25-9)

Guidance literature:

α,α'-dibromo-di-p-tolylamine; With potassium hydride; In tetrahydrofuran; at 20 ℃; Cooling;

benzyl bromide; In tetrahydrofuran; at 20 ℃; for 48h; Cooling;

DOI:10.1021/ic302506e

upstream raw materials:

di-p-tolylamine

Downstream raw materials:

N,N-bis(2-bromo-4-methylphenyl)methylamine

2,2'-Dicyano-4,4'-dimethyldiphenylamin

bis-(2-diisopropylphosphanyl-4-methyl-phenyl)-methyl-amine

2,5,8-trimethyl-10,10-diphenyl-5,10-dihydro-phenazasiline